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《Journal of The Chinese Ceramic Society》 1992-05
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STUDY OF SILICA GLASS DOPED WITH FLUORINE

Gao Sijian Gu Zhenan(China Building Materials Academy)  
By using ammonium fluorine (NH_4F) as a fluorine doping source, silica glass doped with fluorine is prepared through the sol-gel process. Introduction of freon (CCl_2F_2) into the sintering atmosphere increases the amount of retained fluorine in the silica glass up to 2.5%(wt). Refractive index and density of the glass decrease linearly with fluorine content in the glass. Fluorine anion is favorable to the preparation of bulk silica glass. Silica glass doped with fluorine was investigated by IR and Raman spectra, and the results obtained allowa model to be proposed for dopant incorporation in the silica network, involving the formation of [SiO_3F] tetrahedron.
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