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《Journal of The Chinese Ceramic Society》 2004-08
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SYNTHESIS OF β-SIALON UITRAFINE POWDER BY SOL-GEL AND REDUCTION-NITRIDATION METHOD

JIA Xiaolin, ZHANG Haijun, CHEN Junfeng, YANG Daoyuan, LIU Zhanjie (Henan Key Laboratory of High Temperature Ceramics, Zhengzhou University, Zhengzhou 450052, China)  
With aluminium nitrate,silicon ethoxide,alcohol and sucrose etc. as starting materials, ultrafine βsialon powders were prepared by using solgel reductionnitridation processing. The influences of crystal seeds(βsialon, Si_(3)N_(4) and AlN), additives and nitridation temperature on the formation of βsialon were investigated. The results show that the seeding can promote the formation of βsialon and lowering the crystallization temperature. The effect of the amount of crystal seeds added on the crystallization of βsialon is insignificant, but the kind of crystal seeds (βsialon, Si_(3)N_(4) and AlN) is an important factor for βsialon formation. Among which βsialon seeds play the most effective role on the formation of βsialon. It shows that the temperature range of 1 450-1500 ℃ is a suitable nitridation temperature for βsialon preparation. The result of SEM indicates that the particle size of βsialon is about 300 nm, and the hydrolyzation of sialon, Si_(3)N_(4)and AlN are also discussed.
【Fund】: 河南省高校青年骨干教师资助项目 ;; 湖北省耐火材料与高温陶瓷重点实验室省部共建国家重点实验室培育基地开放基地基金资助项目 (G0 40 7)。
【CateGory Index】: TB44
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