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《Journal of The Chinese Ceramic Society》 2004-09
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STATUS AND ENTRANCE MECHANISM OF CALCIUM AND PHOSPHATE IN MICROARC OXIDATION LAYER ON TITANIUM

 HUANG Ping , XU Kewei, HAN Yong ersity, Xi′an710049, China)  
A porous TiO_2 ceramic layer containing calcium and phosphate was prepared by microarc oxidation on titanium. The microstructure, compositions and elements of the ceramic layer were analyzed by SEM, XRD, IR and XPS. The results show that anatase and rutile are the main composition of the layer. With the increasing of applied voltage and Ca~(2+) concentration of (electrolyte), the content of rutile increases. Under high voltage calcium comes into the layer and forms CaTiO_(3), while phosphate comes into the layer and exists as PO_4~(3-). They are homogeneously distributed on the ceramic layer.Diffusion and electrophoresis are the entrance mechanism for calcium and phosphate.
【Fund】: 陕西省攻关计划重点项目(2000K-G1);; 国家自然科学基金(50002008);; 863计划(2002AA326070)资助项目
【CateGory Index】: R318.08
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