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《Journal of the Chinese Ceramic Society》 2007-03
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MECHANISM OF MODIFICATION OF SILANE COUPLING AGENTS AND PROPERTIES OF MODIFIED SERICITE

XUE Rujun 1,2,WU Yucheng 1(1.School of Materials Science and Engineering,Hefei University of Technology,Hefei 230009;2.Department of Chemical Engineering,Anhui University of Science and Technology,Huainan 232001,Anhui,China)  
Surface modification of ultra-fine sericite with silane coupling agents(SCA)KH550 and KH570 was carried out.It was shown by IR that the sericite was modified by silane coupling agents compounded with the Si—OH of sericite.The optimum coupling reaction conditions were determined by difference scanning calorimetry-thermogravimetric analysis.The optimum coupling reaction conditions:mass fraction of SCA is 6.5%—7.5%;coupling temperature is 70℃;coupling time is 3—4 h.The dispersivity and stability of modified sericite in organic phase were investigated as well.The test results show that the dispersivity and stability of modified sericite in organic phase are improved,and the oil-absorbing value of modified sericite raises from 0.71 g/g to 1.33 g/g,which is a significant increase.
【Fund】: 合肥工业大学中青年创新群体基金(103-037016);; 安徽省科技攻关项目(06012091B)资助项目
【CateGory Index】: TB39
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