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《Guangzhou Chemical Industry》 2014-14
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Determination of Polychlorinated Biphenyls and Organochlorinated Pesticides in Mussel by Gas Chromatography

SUN Xiu-mei;HU Hong-mei;ZHONG Zhi;JIN Yan-jian;CHEN Xue-chang;HE Yi-na;GUO Yuan-ming;Marine Fishery Institute of Zhejing Province,Key Laboratory of Sustainable Utilization of Technology Research for Fishery Resource of Zhejiang Province;  
A gas chromatography method was developed and validated for determination of polychlorinated biphenyls(PCBs) and organochlorinated pesticides(OPCs) in mussel based on ultrasonic-assisted extraction and solid phase extraction as a clean-up procedure.The biological samples were extracted ultrasonically with hexane,and treated with sulfuric acid,followed by clean-up with solid phase extraction column containin octadecyl silica gel and florisil.The method realized complete base-line separation of the PCBs and OPCs and high sensitive determination based on optimization of gas chromatographic conditions,the temperature program and selected ion monitoring.Under optimizing conditions,the detection limits for PCBs and OCPs were 0.01 ~ 0.04 μg /kg and 0.039 ~ 0.24μg /kg,respectively,the calibration curves of the PCBs and OPCs were linear in the range of 2.5 ~ 100 μg /L with correlation coefficients not less than 0.995.The recoveries at the spiked amount of 1.0 μg /kg,10.0 μg /kg and 100.0 μg /kg were 75% ~ 115%(RSD 15%).The reproducible,sensitive and accurate method was suitable for quality control of the PCBs and OCPs in mussel.
【Fund】: 浙江省科技计划项目(2012F20026);; 浙江省公益性分析测试科技计划项目(2013C37088)
【CateGory Index】: O657.71;TS254.7
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