Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Guangzhou Chemical Industry》 2014-14
Add to Favorite Get Latest Update

Determination of Polychlorinated Biphenyls and Organochlorinated Pesticides in Mussel by Gas Chromatography

SUN Xiu-mei;HU Hong-mei;ZHONG Zhi;JIN Yan-jian;CHEN Xue-chang;HE Yi-na;GUO Yuan-ming;Marine Fishery Institute of Zhejing Province,Key Laboratory of Sustainable Utilization of Technology Research for Fishery Resource of Zhejiang Province;  
A gas chromatography method was developed and validated for determination of polychlorinated biphenyls(PCBs) and organochlorinated pesticides(OPCs) in mussel based on ultrasonic-assisted extraction and solid phase extraction as a clean-up procedure.The biological samples were extracted ultrasonically with hexane,and treated with sulfuric acid,followed by clean-up with solid phase extraction column containin octadecyl silica gel and florisil.The method realized complete base-line separation of the PCBs and OPCs and high sensitive determination based on optimization of gas chromatographic conditions,the temperature program and selected ion monitoring.Under optimizing conditions,the detection limits for PCBs and OCPs were 0.01 ~ 0.04 μg /kg and 0.039 ~ 0.24μg /kg,respectively,the calibration curves of the PCBs and OPCs were linear in the range of 2.5 ~ 100 μg /L with correlation coefficients not less than 0.995.The recoveries at the spiked amount of 1.0 μg /kg,10.0 μg /kg and 100.0 μg /kg were 75% ~ 115%(RSD 15%).The reproducible,sensitive and accurate method was suitable for quality control of the PCBs and OCPs in mussel.
【Fund】: 浙江省科技计划项目(2012F20026);; 浙江省公益性分析测试科技计划项目(2013C37088)
【CateGory Index】: O657.71;TS254.7
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 8 Hits
1 Zhao Rongbiao,Qin Zhanfen,Zhao Rusong,Xu Xiaobai~ (State Key Laboratory of Environmental Chemistry and Ecotoxicology,Research Center for Eco-Environmental Sciences,Chinese Academy of Sciences,Beijing 100085);Studies on Analytical Method for Trace Polychlorinated Biphenyls Congeners in the Xenopus Laevis and Feeding Water[J];Chinese Journal of Analytical Chemistry;2005-10
2 HE Shan-shan 1,CAO Ling 1,2*,WANG Yan-xin 1,3, DONG Chuang-ju 2,LIN Cong-hui 2(1.School of Environmental Studies,China University of Geosciences;2.Faculty of Material Science and Chemistry, China University of Geosciences;3.State Key Lab of Biogeology and Environmental Geology,China University of Geosciences,Wuhan 430074,China);Organochlorine Pesticides Residues in Top Soil of Central Jianghan Plain:Sources and Distribution Pattern[J];Environmental Science & Technology;2013-02
3 Hua Xiaomei Shan Zhengjun (Nanjing Institute of Environmental Sciences,NEPA,Nanjing 210042);THE PRODUCTICN AND APPLICATION OF PESTIDICES AND FACTOR ANALYSIS OF THEIR POLLUTION IN ENVIRONMENT IN CHINA[J];Advances in Environmental Science;1996-02
4 FEI Yong,et al.(Huzhou Environmental Monitoring Centre,Huzhou 313000,China);Determination of 36 Kind of PCBs&OCPs in Fish by GPC and GC/ECD[J];Environmental Monitoring in China;2011-02
5 WU Jinhao1,2 LI Ai1,2 LIU Guiying1,2 WANG Nianbin1,2(1.Liaoning Ocean and Fishery Science Research Institute,Dalian,116023,China; 2.Liaoning Ocean Environment Monitoring Station,Dalian,116023,China);Determination of polychlorinated biphenyls and organochlorine pesticide residues in wakame by gas chromatography with electron capture detection using microwave-assisted extraction[J];Environmental Chemistry;2013-01
6 TIAN Haizhen1,2 WANG Ling1 GAO Lirong2 ZHANG Bing2 LI Cheng2 LIU Lidan2 LIU Zhitong2 ZHANG Wenjing3(1.Faculty of Science,Agricultural University of Hebei,Baoding,071001,China; 2.Research Center for Eco-Environmental Sciences,Chinese Academy of Sciences,Beijing,100085,China; 3.School of Safety and Environmental Engineering,Capital University of Economics and Business,Beijing,100026,China);Distribution of organochlorine pesticides(OCPs) in the surface sediments of Zhujiang River[J];Environmental Chemistry;2013-02
7 MA Zi-long,MAO Xiao-xuan,DING Zhong-yuan,GAO Hong,HUANG Tao,TIAN Hui,GUO Qiang(College of Earth and Environmental Sciences,Lanzhou University,Lanzhou 730000,China);Residual Levels in Air,Soil and Soil-Air Exchange of Organochlorine Pesticides in Hami Region of Xinjiang and Its Potential Ecological Risk[J];Environmental Science;2013-03
8 LU Xianbo,CHEN Jiping*,WANG Shuqiu,ZOU Lili,TIAN Yuzeng,NI Yuwen,SU Fan( Dalian Institute of Chemical Physics,Chinese Academy of Sciences,Dalian 116023,China );Preparation and certification of mussel reference material for organochlorine pesticides and polychlorinated biphenyls using isotope dilution-high resolution mass spectrometry[J];Chinese Journal of Chromatography;2012-09
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 LIAO Jian-liang et al(Department of Biology,Huizhou University,Huizhou,Guangdong 516015);Investigation of the Residues of Organic Phosphorous Pesticide in Chinese Cabbage[J];Journal of Anhui Agricultural Sciences;2006-02
2 MA Feng-xia et al(College of Arts and Science,Jilin Agricultural Science and Technology University,Jilin,Jilin 132101);Study on Photo Catalyzing Degradation of Organophosphorous Pesticides by Polyoxometalates[J];Journal of Anhui Agricultural Sciences;2009-10
3 CAO Jing et al(College of Agronomy,Liaocheng University,Liaocheng,Shandong 252059);Research on the Formula of 5% Acetamiprid EC[J];Journal of Anhui Agricultural Sciences;2009-12
4 HU Chun-hua et al(Key Lab of Lake Ecology and Bio-resource Utilization of Poyang Lake,Ministry of Education,Nanchang University,Nanchang,Jiangxi 330029);Residual Characteristic and Eco-risk Assessment of DDT in Differently Using Types Soil in Jiangxi Province[J];Journal of Anhui Agricultural Sciences;2010-05
5 LI Yue-ru et al(Ginseng and Antler Products Testing Centre of the Ministry of Agriculture PRC,Jilin Agricultural University,Changchun,Jilin 130118);Residual Analysis of Iprodione in Ginseng and Soil[J];Journal of Anhui Agricultural Sciences;2012-19
6 ZHU De-long,YANG Chun-yan(Environmental Monitoring Center of Huludao City,Huludao 125000,China);Current situation and countermeasures of rural non-point source pollution[J];Journal of University of Science and Technology Liaoning;2010-04
7 ZHANG Xiang-zhu~1,WU Ming-shu~2(1.Anyang University,Anyang 455000,China;2.Anyang County Environmental Protection Bureau,Anyang 455000,China);On Modern Technology of Agricultural Chemicals and Sustainable Development of Ecological Environment[J];Journal of Anyang Teachers College;2004-05
8 Yang Kangzhen Zhang Yun Li Jieli You Jiming Li Hongmei Han Hua Zhang Congwen;Progress in Determination Method of BHC and DDT Residues in Food Samples[J];Beijing Agriculture;2012-09
9 HU Hong_tao,LIN Xue_yu,LIAO Zi_sheng,ZHANG Lan_ying, JIANG Gui_lan,LIU Guang_min,WEI Li_hong (College of Environment and Construction Engineering, Jilin University, Changchun 130026,China);EXPERIMENTAL STUDY ON MIGRATION OF ATRAZINE IN GROUNDWATER[J];Journal of Changchun University of Science and Technology;2001-03
10 HU Hong tao 1,LIN Xue yu 2,LIU Na 2,LI Li 2 (1 School of Environmental Science and Engineering, Tongji University, Shanghai 200092,China; 2 School of Environment and Resource, Jilin University, Changchun 130026,China);Experimental Research on Characteristic of Growth and Its Degradation of Bacteri um AT[J];Urban Environment & Urban Ecology;2003-03
China Proceedings of conference Full-text Database 4 Hits
1 WANG De-chun JIN Ping JIN Su Danisco(China)Co.Ltd.,Shanghai 200335,China;Research on the Fermented Apple Juice Using Kefir Grain Starter[A];[C];2008
2 LI Dong-mei~1 LI Jian-ke~1 SHI Zhi-cheng~2 (1 Department of Food Engineering,Shaanxi Normal University,Xi'an 710062; 2 Institute of Eco-Toxicology in Northwest University,Xi'an 710069);Toxicological Hazard of Persistent Organic Pollutants(POPs) and Its Environmental Pollution Control[A];[C];2007
3 LI Dong-mei~(1,2),LI Jian-ke~(1*),SHI Zhi-cheng~3,LI jun-jian~2 (1 College of Food Science,Shaanxi Normal University,Xi'an 710069,China; 2 Xi'an Agriculture Science Research Institute,Xi'an 710061,China; 3 College of Life Science,Northwest University,Xi'an 710069,China);Solid-phase Extraction and Gas Chromatography Determination of Persistent Organic Pollutants in soil[A];[C];2008
4 ;高效液相色谱法测定饮料中的合成着色剂[A];[C];2008
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 ZHOU Lin~1 CHEN Da-zhou~2 SHEN Yan-hua~1 LI Lei~1(1.College of Science,Beijing University of Chemical Technology,Beijing 100029;2.National Research Center For CRM'S,Beijing 100013,China);Extraction of PCBs in shellfish by accelerated solvent extraction[J];Journal of Beijing University of Chemical Technology;2005-05
2 SU Qiu-ke1a,1c,QI Shi-hua1b,1c,WU Chen-xi1a,1c,HU Li-song2,WANG Wei1a,1c,Ellis Burnet Julia1b,1c,GONG Xiang-yi1a,1c,LU Chun-ling1a,1c,LIU Hua-feng1a,1c(1a.Graduate School;1b.School of Environmental Studies;1c.Key Laboratory of Biogeologyand Environmental Geology of Ministry of Education,China University of Geosciences,Wuhan 430074,China;2.School of Environmental and Civil Engineering,Wuhan Instituteof Technology,Wuhan 430073,China);Organism Productions Accumulating Model of Organochlorine Pesticides in Water and Sediments from Honghu Lake,Hubei Province,China[J];Geological Science and Technology Information;2007-04
3 SHI Shuangxin1, LU Wanyun2, SHAO Dingding1, ZHOU Li1, ZHANG Ting1 & HUANG Yeru1 (1: National Research Center for Environmental Analysis and Measurements, Dioxins Laboratory of the National Research Center for Environment Analysis and Measurement, Beijing 100029, P.R.China) (2: Environment College, Renmin University of China, Beijing 100081, P.R.China);Determination of organochlorine pesticides in wild shrimps muscle tissue in Lake Taihu and Lake Dongting by Gas Chromatogrphy/Mass Spectrometry[J];Journal of Lake Sciences;2009-05
4 Li He, Li Gongke *, Zhang Zhanxia (School of Chemistry and Chemical Engineering, Sun Yat-sen University, Guangzhou 510275);Development of Microwave Assisted Extraction[J];Chinese Journal of Analytical Chemistry;2003-10
5 Gao Lirong~1,Zheng Minghui~(*1),Li Jingguang~2,Zhang Bing~1,Liu Wenbin~1,Zhao Xingru~1,An Fengchun~1,Fang Liping~1,Wu Yongning~2~1(Research Center for Eco-Environmental Science,Chinese Academy of Sciences,Beijing 100085)~2(Institute of Nutrition and Food Hygiene,Chinese Center for Disease Control and Prevention,Beijing 100050);Preparation,Testing and Certification of Soil Reference Materials for Polychlorinated Biphenyls[J];Chinese Journal of Analytical Chemistry;2006-11
6 Fang Jie1,2, Wang Kai-Xiong1,31(Department of Environmental Engineering, College of Environmental and Resource Sciences, Zhejiang University, Hangzhou 310029)2(Zhejiang Zhoushan Marine Ecological Environmental Monitoring Station, Zhoushan 316004)3(College of Biology and Environmental Engineering, Zhejiang Shuren University, Hangzhou 310015);Multiresidual Analysis of Organochlorine Pesticides, Polychlorinated Biphenyls and Polycyclic Aromatic Hydrocarbons in Marine Shellfishes by Gas Chromatography-Ion Trap Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2007-11
7 SUN Cheng XU Shi-fen YAO Shu-chun WANG Lian-sheng (State Key Laboratory of Pollution Control and Resource Reuse,School of the Environment,Nanjing University,Nanjing,210093) CHIU Sein Tuck YE Ding-yi CHAU Oliva (Department of Biology,Hong Kong Baptist University,Kowloon Tong,Hong Kong,China);STUDY ON PCBs IN THE GREEN MUSSEL(PERNA VIRIDIS L.) SAMPLES IN HONG KONG MARINE WATER[J];Environmental Chemistry;2003-02
8 WANG Jun1,2,5 ZHANG Gan1 LI Xiang-dong3 LI Jun1 XU Wei-hai1 GUO Ling-li1 YU Li-li1 ZHONG Liu-ju4 XIANG Yun-rong4 PENG Rong-zhuo4(1 State Key Laboratory of Organic Geochemistry,Guangzhou Institute of Geochemistry,Chinese Academic of Sciences,Guangzhou,510640,China;2 Institute of Hydrobiology,Jinan University,Guangzhou,510632,China;3 Department of Civil and Structural Engineering,the Hong Kong Polytechnic University,Hong Kong,China;4 Environmental Protection Monitoring Centre of Guangdong Province,Guangzhou,510045,China,5 Graduate University of Chinese Academy of Sciences,Beijing,100039,China);PASSIVE AIR SAMPLING SURVEY OF ORGANOCHLORINE PESTICIDES IN THE PEARL RIVER DELTA[J];Environmental Chemistry;2007-03
9 CHEN WeiSONG QiLIU MengEllis Burnet JuliaQI Shi-hua (Key Laboratory of Biogeology and Environmental Geology of MOE,School of Environmental Studies,China University of Geosciences,Wuhan,430074,China);DISTRIBUTION AND RISK ASSESSMENT OF ORGANOCHLORINE PESTICIDES IN SURFACE SEDIMENT FROM THE PEACOCK RIVER IN XINJIANG,CHINA[J];Environmental Chemistry;2009-02
10 LIU Lidan1,2 WANG Ling1 GAO Lirong 2 LI Cheng2 ZHANG Bing2 LI Sumei2 HUANG Wenjun3 ZHOU Xin4 LI Yao4(1.College of Science,Agricultural University of Hebei,Baoding,071001,China;2.Research Center for Eco-Environmental Sciences,Chinese Academy of Sciences,Beijing,100085,China;3.Institute of Urban Environment,Chinese Academy of Sciences,Xiamen,361021,China;4.College of Resources and Civil Enginceering,Northeastern University,Shenyang,110004,China);OCCURRENCE AND DISTRIBUTION OF ORGANOCHLORINE PESTICIDES(OCPs) IN SURFACE SEDIMENTS OF THE YA-ER LAKE IN HUBEI PROVINCE,CHINA[J];Environmental Chemistry;2011-09
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved