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《Strait Pharmaceutical Journal》 2012-03
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Study on preparing technique and quality standards of Guiling granules

CHEN Qian-jin1,FANG Dan-kai2,RUAN Wei-wan1(1.Taishan Hospital of TCM,Guangdong,Taishan 529200,China;2.Jiangmen Hengjian Pharmaceutical Factory,Jiangmen 529000,China)  
OBJECTIVE To study the preparing technique of Guiling Granules and its quality standards.METHODS The best method of extract process was optimized by orthogonal text.Astragaloside IV in Guiling Granules were identified by TLC and the content was determinated by HPLC-ELSD.RESULTS The best method of extraction technique for turtleback was as follows:as the comminuted degree was 20~40 items;adding 8 times of water;extract 3 times;l.5 hours every times.The determination of astragaloside IV:the linear range of flavonoids in astragaloside IV was 0.30~6.0μg,the regression equation:Y=1.6233X-3.5678,r=0.9979(n=5),the average recovery was 97.9% with RSD 1.52%(n=6).Quatilative and quantitative methods are feasible.CONCLUSION The preparing technique of this preparation is reasonable,and its method of quality control is accurate.
【CateGory Index】: TQ461;R286
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