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《Chemistry & Bioengineering》 2006-04
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Synthesis of 3-Methylcyclohex-2-en-1-one and(±)3-Methylcyclohex-2-en-1-ol and Measurement on Bioactivity

YIN Cai-xia~(1),GAO Zhu-lin~(1),LIU Fu-chu~(1),L(U)·· Jun~(2)(1.Department of Applied Chemistry,Yunnan University,Kunming 650091,China;2.College of Life Science,Yunnan University,Kunming 650091,China)  
Using acetylacetic ether and triformol,or anchoic acid as raw material,3-methylcyclohex-2-en-1-one and(±)-3-methylcyclohex2-en-1-ol were synthesized.The structures of the compounds were confirmed by IR、~1HNMR、~(13)CNMR and MS.The two different synthetic routes were compared and the influential factors were discussed.And the response of Tomicus piniperda to 3-methylcyclohex-2-en-1-one and(±)-3-methylcyclohex-2-en1-ol was tested.
【Fund】: 云南省科委攻关项目(2001NC30)
【CateGory Index】: O624.3
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