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《Chinese Journal of Synthetic Chemistry》 2007-03
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Synthesis of Chiral 1,3,4-Oxadiazole Thioether Derivatives

MA Yin-jian,ZHU Hong,LI Xue-qiang(a.Key Laboratory of Energy Sources and Chemical Engineering;b.Development Center of Natural Products and Medication;c.Department of Chemistry and Chemical Engineering,1.Ningxia University,Yinchuan 750021,China)  
Six novel chiral 1,3,4-oxadiazole thioether derivatives in yields of 55%~67% were synthesized by Michael addition-elimination reactions of 5-substituted-2-mercapto-1,3,4-oxadiazoles(as a nucleophile) and chiral 5-(l-menthyloxy)-3,4-dibromo-2(5H)-furanone.The structures were characterized by 1H NMR,13C NMR,IR and HR-MS.
【Fund】: 宁夏自然科学基金资助项目(NZ0606);; 宁夏教育厅自然科学基金资助项目(2005);; 宁夏大学自然科学基金资助项目(2001);; 宁夏大学能源化工重点实验室开放基金资助项目(2004)
【CateGory Index】: O626.2
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