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《Journal of Henan University(Natural Science)》 2011-02
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Effect of the Nano Nickel Shapes on the Catalytic Activity for Suzuki-Miyaura Coupling Reaction

ZHANG Yan-hua,LIU Xiang-yun,TIAN Da-min(Department of Chemistry and Chemical Engineering,Henan University of Urban Construction,Henan Pingdingshan 467044,China)  
Nano nickel with different shapes were synthesized starting from Nickel(II) acetate tetrahydrate and using sodium borohydride or hydrazine hydrate as reductants in the presence of PVP or SDS as modifiers,the organic solvent is ethylene glycol.The catalytic activity was colsely related to the shapes of nano nickel for the Suzuki-Miyaura coupling reaction.The shapes were characterized by transmission of electron microscopy and X-ray diffraction.The products were determined by 1HNMR,13CNMR and MS.
【Fund】: 河南省科技厅科技攻关项目(072102230035)
【CateGory Index】: TB383.1
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