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《New Chemical Materials》 2008-11
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The conductivity and structural characterization of H_2SO_4 doping polyaniline/attapulgite nanocomposites

Zeng Yongbin1 Yao Chao1 Ding Yonghong1 Li Xiaotang2 Liu Jianping3(1.Department of Chemical Engineering,Jiangsu Polytechnic University,Changzhou 213164;2.Jiangsu Engineering Technology Research Center of Attapulgite,Xuyi 211700;3.Jiangsu NDZ Technology Co.Ltd.,Changzhou 213016)  
The surface of attapulgite was encapsulated with polyaniline(PANI) which doped with sulfuric acid(H2SO4) to synthesize the H2SO4-PANI/ATP nanocomposites by in situ polymerization method.The effect of the polymerization temperature,the covering ratio of aniline,the amount of H2SO4,the polymerization time and the amount of Ammonium persulfate(APS) on the volume resistivity were studied.The result indicated that the volume resistivity of nanocomposites could reach 3Ω·cm when the polymerization temperature was 20℃,the covering ratio of aniline was 30%,the polymerization time was 4h,the molar ratio of An,APS and H2SO4 was 1∶1∶7.76.The nanocomposites prepared on this condition were also characterized by TG-DTA,XRD and FTIR.
【Fund】: 国家863项目(2007AA06Z118);; 江苏省科技攻关(No.BE2006373 No.BE2006045);; 江苏省博士后基金(No.0602020B);; 常州市科技攻关(No.CE2007075)资助项目
【CateGory Index】: TB383.1
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