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《Hebei Chemical Engineering and Industry》 2010-08
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Determination of Lead in Ferrosilicon by Sequential Injection Hydride Generation Atomic Fluorescence Specttrometry

SHI Cun-jie1,WANG Zheng-hua2,GUO Zu-peng1,YAN Hai-bo1(1.Chemical Engineering College,Qinghai University,Xining 810016,China;2.New Energy Branch,Qinghai Huanghe Hy-dropower Development Co.,Ltd,Xining 810008,China)  
A method of injection hydride generation combined with atomic fluorescence spectrometry for the determination of Pb in ferrosilicon was reported in this paper.The sample was digested with HNO3-HF-HClO4.Under the selected condi-tions,recovery of the method was in range of 95%~106%,detection limit was 0.410 3 ng/mL and RSD was 1%~5%.
【CateGory Index】: TG115.33
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