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《The Administration and Technique of Environmental Monitoring》 2009-01
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Determination of Metals in Atmospheric Particles by Inductively Coupled Plasma Atomic Emission Spectrometry with Microwave Digestion

DENG Ji1,CHEN Guo-hai2,ZHENG Xiao-hong2,CHEN Feng2,MA Wei2,LIU Fang2(1.East China University of Science and Technology,Shanghai 200237,China;2.Shanghai Environment Monitoring Center,Shanghai 200030,China)  
The method was established for determining lead,nickel,chromium,copper,iron,zinc,manganese,barium and cadmium in atmospheric particulates by ICP-AES with microwave digestion and perchloroethylene filter collection of the samples.The experimental conditions were optimized to produce the following results: good linearity,the detection limits of all elements from 0.001 mg/L to 0.01 mg/L,the RSDs of the filter samples from 0.6% to 2.9%,the recoveries from 96.0% to 105%.
【CateGory Index】: X831
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