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《The Administration and Technique of Environmental Monitoring》 2009-03
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Simultaneous Analysis of 7 Antibiotics in Water by Ultra Performance Liquid Chromatography-Electrospray Ionization-Tandem Mass Spectrometry

ZHANG Chuan1,HU Guan-jiu1,2,SUN Cheng1(1.The State Key Lab of Pollution Control and Resource Reuse,School of the Environment,Nanjing University,Nanjing,Jiangsu 210093,China;2.Jiangsu Province Environmental Monitoring Centre,Nanjing,Jiangsu 210036,China)  
An ultra performance liquid chromatography-electrospray ionization-tandem mass spectrometry(UPLC-ESI-MS/MS) analysis method was established for the simultaneous analysis of7 antibiotics in water.The experimental conditions were optimized to produce following results: good linearity of sulfamethoxazole,norfloxacin,ciprofloxacin,ofloxacin and tetracycline in the range from 1.00 ng/L to 1 000 ng/L and the limits of quantification(LOQ) 1 ng/L,the good linearity of terramycin and aureomycin in the range from 10.0 ng/L to 2 000 ng/L and the LOQ 10 ng/L,the recoveries of deionized water and surface water from 72.1% to 112%,and the RSD from 0.6% to 9.2%.
【Fund】: 江苏省环境监测科研基金资助项目(0613)
【CateGory Index】: X832
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