Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《The Administration and Technique of Environmental Monitoring》 2009-03
Add to Favorite Get Latest Update

Simultaneous Analysis of 7 Antibiotics in Water by Ultra Performance Liquid Chromatography-Electrospray Ionization-Tandem Mass Spectrometry

ZHANG Chuan1,HU Guan-jiu1,2,SUN Cheng1(1.The State Key Lab of Pollution Control and Resource Reuse,School of the Environment,Nanjing University,Nanjing,Jiangsu 210093,China;2.Jiangsu Province Environmental Monitoring Centre,Nanjing,Jiangsu 210036,China)  
An ultra performance liquid chromatography-electrospray ionization-tandem mass spectrometry(UPLC-ESI-MS/MS) analysis method was established for the simultaneous analysis of7 antibiotics in water.The experimental conditions were optimized to produce following results: good linearity of sulfamethoxazole,norfloxacin,ciprofloxacin,ofloxacin and tetracycline in the range from 1.00 ng/L to 1 000 ng/L and the limits of quantification(LOQ) 1 ng/L,the good linearity of terramycin and aureomycin in the range from 10.0 ng/L to 2 000 ng/L and the LOQ 10 ng/L,the recoveries of deionized water and surface water from 72.1% to 112%,and the RSD from 0.6% to 9.2%.
【Fund】: 江苏省环境监测科研基金资助项目(0613)
【CateGory Index】: X832
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【Citations】
Chinese Journal Full-text Database 3 Hits
1 ;Quality Control in Determination of VOC and SVOC in Water with InternalStandard Method by GC/MS[J];THE ADMINISTRATION AND TECHNIQUE OF ENVIRONMENTAL MONITORING;1999-03
2 Ding Zhigang~1 Wang Jing~2 He Shu~2 1(Institute of Technology, Anhui Science and Technology University, Bengbu, 233100,China) 2(Chinese Academy of Agricultural Sciences, Beijing, 100081, China);Research Advance on Detection Technique of Residual Antibiotics[J];Food and Fermentation Industries;2005-06
3 QIN Yan, ZHANG Meijin, LIN Haidan(Guangzhou Entry & Exit Inspection and Quarantine Bureau, Guangzhou 510623, China);Qualification and Quantification of 10 Sulfonamides in Animal Feedstuff by High Performance Liquid Chromatography-Electrospray Tandem Mass Spectrometry[J];Chinese Journal of Chromatography;2005-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 YI Li et al(Life Science College,Luoyang Normal University,Luoyang,Henan 471022);Effects of Kitasamycin on Microbial Community in Weaning Pigs' Intestinal Tract[J];Journal of Anhui Agricultural Sciences;2006-01
2 DAI Chang-chun(Binzhou Vocational College,Binzhou,Shandong 256603);Sulfaquinoxaline Chick Intoxication Experiment[J];Journal of Anhui Agricultural Sciences;2007-20
3 YANG Jie,XIA Hong,MENG Di-ya(Food Quality Supervision Inspection and Testing Center of Agr Ministry,Wuhan 430064,China);Simultaneous Determination of Five Sulfonamides and Three Tetracyclines In Animal Source Food by High Performance Liquid Chromatograpy[J];Analysis and Testing Technology and Instruments;2006-03
4 FU Ruo-nong(Department of Chemistry,Beijing Institute of Technoligy,Beijing 100081);Advances on SPE-chromatography in China in recent two years[J];Chinese Journal of Analysis Laboratory;2007-02
5 ZHANG Yi-jun1,WANG Min-can1,ZHANG Shu-sheng1,ZHANG Yu-ping2 and ZHENG Ming-ming1(1.Department of Chemistry,Zhengzhou University,Henan 450001;2.Henan Institute of Science and Technology,Henan 453003);Application of response surface methodology in optimizing separation of sulfonamides by high performance liquid chromatography[J];Chinese Journal of Analysis Laboratory;2007-12
6 DAN De-zhong,YAO Yu-ling and JIANG Wen-jing(Department of Environmental Science and Engineering,Sichuan University,Chengdu 610065);Analysis of environmental samples[J];Chinese Journal of Analysis Laboratory;2008-04
7 MAO Bin,HAN Gen-liang,LI Gong-nong,LIU Guo-han(Institute of Sensor Technology,Gansu Academy of Sciences,Lanzhou 730000,China);The Application of Biosensor to Detect the Pesticide and Antibiotics Leftover in Food[J];Journal of Gansu Sciences;2007-02
8 ZHU Xiao-lei1,2,3, LI Zhan-chen1, KANG Quan-ying2,3, WANG Jing-fei2,3, TIAN Zai-feng2,3 (1. College of Chemistry and Environmental Science,Hebei University,Baoding 071002,China; 2. Hebei Provincial Labo- ratory of Water Environmental Science,Hebei Provincial Academy of Environmental Science,Shijiazhuang 050051,China;3. Na- tional Environmental Protection Engineer Technical Center of Pharmaceutical Wastewater Pollution Control,Shijiazhuang 050051,China);Detection of Oxytetracycline Residues in Pharmaceutical Wasterwater by SPE-HPLC[J];Hebei Chemical Engineering and Industry;2008-12
9 WANG Peng-hua, YUAN Tao, TAN You-ming. Department of Environmental Science and Engineering, Shanghai Jiaotong University, Shanghai 200240, China;Effects of Pharmaceuticals Pollution in the Aquatic Environment on Aquatic Organism and Human Health[J];Journal of Environment and Health;2008-02
10 WANG Peng-hua~1,et al(1.Department of Environmental Science & Engineering;Shanghai Jiao Tong University,Shanghai 200240,China);Screening the Priority Control Pharmaceuticals in the Aquatic Environment[J];Environmental Monitoring in China;2008-04
China Proceedings of conference Full-text Database 1 Hits
1 Ye Sai, Yang Mei, Zhang Kui-wen, Na Guang-shui, Yao Zi-wei, Wang Ju-ying, Ma De-yi National Marine Environmental Monitoring Center, 116023; College of Environmental Science and Engineering, Dalian Maritime University, 116026; Dalian Fishery University, 116023;Simultaneous Determination of 14 Sulfonamides in Wastewater by Liquid Chromatography-Tandem Mass Spectrometry[A];[C];2006
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 LU Wan-hua, CHEN Tian-bao, DENG Wen-han, CHEN Ru-ming, RAO Ping-fan (Institute of Biotechnology, Fuzhou University, Fuzhou, Fujian 350002, China);Separation of antibiotics with capillary electrophoresis[J];JOURNAL OF FUZHOU UNIVERSITY(NATURAL SCIENCES EDTION);2000-05
2 FANG Yu-Zhi; FANG Xiao-Ming; YE Jian-Nong (Department of Chemistry, East China Normal University, Shanghai, 200062);Determination of Polyhydroxy Antibiotics by Capillary Electrophoresis with Amperometric Detection at a Copper Electrode[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;1995-10
3 Wei Aixue(Research Center for Eco-Environmental Siences, Chinese Academy of Sciences, Beijing 100085 );QUALITY CERTIFICATION FOR MEASURE VOCIN WATER BY USING EPA-8260 METHOD[J];;1996-03
4 Sun sien et al. (The Research Center for Eco-Environ-mental Sciences, Academia Sinica,Beijing 100085);Quality Control for the Analysis of Volatile Organic Pollutants by GC-MS.[J];Environmental Science;1993-04
5 ;Screening Testing in Milk[J];;2004-10
6 CHEN Tian bao,\ DENG Wen han,\ LU Wan hua,\ CHEN Ru ming,\ RAO Ping fan (Institute of Biotechnology, Fuzhou University, Fuzhou 350002, China);Detection of Residual Antibiotics in Honey with Capillary Electrophoresis[J];Chinese Journal of Chromatography;2001-01
7 JIA Wei, SUN Lu, SHI Xiang guo, CHEN Xiao yan, ZHONG Da fang (Laboratory of Drug Metabolism and Pharmacokinetics, Shenyang Pharmaceutical University, Shenyang 110016, China);Measurement of the four tetracycline residues in the milk by high-performance liquid chromatography mass spectrometry[J];Journal of Shenyang Pharmaceutical University;2002-02
8 Fang Xiaoming Zhang She(Technological Center for Animal, Plant and Food Inspection & Quarantine, Shanghai Exit-Entry Inspection & Quarantine Bureau Shanghai 200135);Recent progress in liquid chromatography-tandem mass spectrometry and its applications[J];Modern Instruments;2002-03
9 Li Xia(Chongqing Institute for Drug Control ,Chongqing,China 400015);Application of the Microbiological Method in Examining the Quality of Antibiotics[J];China Pharmaceuticals;2004-09
10 Chen Baosheng (Institute of Environmental Health and Engineering, Chinese Academy of Preventive Medicine, # 29 Nan Wei Road, Beijing 100050, P. R. China);Internal standard Method for the Quantitative Analysis of semivolatile Organic Compounds in Water[J];Journal of Chinese Mass Spectrometry Society;1993-02
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved