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《Chinese Journal of Environmental Engineering》 2016-12
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Properties and characterization of Cu_xFe_(1-x)@γ-Al_2O_3 catalysts on treating ceramic printing wastewater with catalytic wet oxidation method

ZHOU Yanbo;ZHU Jujian;DAI Shujuan;ZHANG Yongli;School of Mining Engineering,University of Science and Technology Liaoning;School of Chemical and Environmental Engineering,Hanshan Normal University;  
Four catalysts( CuxFe1-x@ γ-Al_2O_3) were prepared using the impregnation method at room temperature,and then applied to treating ceramic printing wastewater with the catalytic wet oxidation method. Experiments were conducted on the impact of composition of the CuxFe1-x@ γ-Al_2O_3 catalyst on wet oxidation activity and stability. The results showed that the Cu0. 5Fe0. 5@ γ-Al_2O_3 catalyst displayed the highest catalytic activity and stability of the four prepared catalysts( Cu0. 5Fe0. 5@ γ-Al_2O_3,Cu@ γ-Al_2O_3,Fe@ γ-Al_2O_3 and γ-Al_2O_3).For the Cu0. 5Fe0. 5@ γ-Al_2O_3 catalyst,iron drives copper to enter the lattices of the γ-Al_2O_3 support and to form a stable solid solution( Al2 Cu O4). Therefore,this catalyst displayed the greatest hardness and stability of the four samples. After being applied for catalytic wet oxidation,the catalyst showed little change in its morphology or crystal phase,which confirmed the stability of the catalyst. Under optimal running conditions,the COD and chromaticity of the ceramic printing wastewater treated by catalytic wet oxidation method,with the catalyst CuxFe1-x@ γ-Al_2O_3,were 280 mg·L~(-1)and 20 times,respectively,which met the third emission standard on dye wastewater,under the Integrated Wastewater Discharge Standard( GB 8978-1996).
【Fund】: 辽宁省工业特种资源行业高新技术研发项目(MYF2012-23);; 2014韩山师范学院教授启动项目(QD20140615)
【CateGory Index】: X781.5
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