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《Research of Environmental Sciences》 2009-04
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Simultaneous Determination of Fifteen Sulfonamide Residues in Macrobenthos by High-Performance Liquid Chromatography Tandem Mass Spectrometry

NA Guang-shui1,ZHOU Chuan-guang1,WANG Zhen1,WANG Qiang1,LI Hong-xia2,CHEN Tong3,ZHANG Yue-mei3,YAO Zi-wei11.National Marine Environmental Monitoring Center,Dalian 116023,China2.College of Life Science and Technology,Dalian Fisheries University,Dalian 116023,China3.College of Biological & Food Technology,Dalian Polytechnic University,Dalian 116034,China  
This study used a rapid method for the determination of 15 kinds of sulfonamides(SAs) in macrobenthos using LLE-SPE,and LC-MS/MS with positive ESI(ESI(+)) and selected reaction monitoring(SRM) mode.The method was applied to quantify the SAs residue in macrobenthos around Dalian.The results showed that sulfathiazole(STZ),sulfathiazole(SQX),sulfadiazine(SDZ) and sulfamethoxazole(SMZ) were frequently found in macrobenthos in a concentration range between 1.39 and 143.29 ng/g.This indicated that there was antibiotics residue in macrobenthos in the sea environment,which threatens the safety of the halobios.Therefore,strengthening the monitoring and managment of antibiotics residues in the sea environment is important.
【Fund】: 国家高技术研究发展计划(863)项目(2007AA09Z126)
【CateGory Index】: X830
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