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《Fine Chemical Intermediates》 2008-05
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One-pot Synthesis of 2,3-Dichloropyridine

FENG Cun1,2,LI Hui2,3,MAO Chun-hui2,YANG Bing2,CHEN Ming2(1.Department of Chemistry,Central China Normal University,Wuhan 430079,China;2.Hunan Research Institute of Chemical Industry(Hunan Research Institute of Pesticide),Changsha 410007,China;3.College of Chemistry and Chemical Engineering Hunan Normal University,Changsha 410081,China)  
2,3-Dichloropyridine is a key intermediate of a new insecticide chlorantraniliprole.Several synthesis routes of 2,3-dichloropyridine were evaluated in this paper,and therefore an economic and reasonable one-pot synthesis of 2,3-dichloropyridine was explored through chlorination,diazotization and sandmeyer reaction starting with 3-aminopyridine yield and purity of the product was 66.9% and 98% respectively.In additions of the mechanisms of reactions were studied and the by-products were separated and characterized.
【CateGory Index】: TQ253.2
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