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《Journal of Nuclear Agricultural Sciences》 2006-05
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MICROSYNTHESIS OF A NOVEL HERBICIDE,PROPYL 4-[2-[(4,6-DIMETHOXY-2-PYRIMIDINYL)OXY] BENZYLAMINO]BENZOATE

YANG Zheng-min~(1,3) YE Qing-fu~2 TANG Qing-hong~3 LU Long~3(1.College of Science,Northwest University of Agriculture and Forestry,Xianyang,Shanxi 712100;2.Institute of Nuclear-Agricultural Science,Zhejiang University,Hangzhou,Zhejiang,ZJ273 310029;3.Shanghai Institute of Organic Chemistry,Chinese Academy of Sciences,Shanghai 200032)  
ZJ273,propyl 4-[2-[(4,6-dimethoxy-2-pyrimidinyl)oxy]benzylamino]benzoate,is a novel herbicide.The microsynthetic method of the compound was developed from 4,6-dimethoxy-2-pyrimidine,propyl(4-benzylamino) benzoate and phenol,and then purified by preparative-HPLC.The yield of end product was 53%.Its chemical structure was characterized by means of()~1H-NMR,MS,UV,and its chemical purity was determined to be exceed 98% by HPLC.The microsynthetic method of propyl 4[2-[(4,6-dimethoxy-2-pyrimidinyl)oxy] benzylamino]benzoate developed sets up a basis to synthesize the radioisotopic labeled target compound.
【Fund】: 国家自然科学基金重点项目(20632070);; 中国科学院知识创新工程方向性项目(KGCX3-SYW-203)
【CateGory Index】: TQ457
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1 Zhang Zongjian and Li Yanghan(Nan jing Agricultural University,Nanjing 210095)Zhang Zhimin(Northwestern Agricultural University,Shaanxi 712100);EFFECT OF PENDIMETHaLIN ON MITOSIS OF MAIZE SEEDLING ROOT MERISTEMATIC CELLS[J];ACTA BOTANICA BOREALI-OCCIDENTALIA SINICA;1995-06
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