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《Synthetic Materials Aging and Application》 2009-02
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Preparation and Characterization of Pure Acrylic Microemulsion

GUO Wen-lu,ZHANG Li(School of Materials Science and Engineering,Jiangsu University of Science and Technology,Zhenjiang 212003,Jiangsu,China)  
The synthesis of pure acrylic microemulsion was prepared by semi-continuous seeded emulsion polymerization,adopting methyl methacrylate,butyl acylate and adding a little methacrylic acid.Then the best formulas were made out.The effects of the ratio of soft and hard monomer,the ratio and the lever of emulsifiers,pH value and polymerization temperature,reaction time in the system on the stability of emulsion polymerization,properties and appearance of latex were discussed.The results showed that when the ratio of hard and soft monomer was 5:4,the ratio of emulsifiers was 4:1,emulsion was 3%,initiatator was 0.5%,pH value was around 7~8,polymerization temperature was 80~88℃,reaction time was 150min,the properties of pure acrylic emulsion and films are the best.The analyzed results of Fourier Transform Infrared Spectroscopy(FTIR) show that the radical copolymerization has happened among the monomers.
【CateGory Index】: O648.23
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