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《Chemical Sensors》 2006-02
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Super-molecule electrochemical sensor for the determination of brucine based on β—cyclodextrin

Liu Shou-qing,Gu Jian-ping,Chen Fei(The Department of Chemistry and Chemical Engineering, University of Science and Technology of Suzhou, Suzhou 215009, China)  
An electrochemical sensor was prepared based on the recognition of β—cyclodextrin for brucine according to the mass ratio of 1∶2 of β—cyclodextrin to carbon powder. The sensor was immersed in a brucine solution first, then taken out, rinsed by distilled water, finally scanned in KCl supporting electrolyte. The anodic current was linearly proportional to the concentration of brucine in the range of 5.0×10-6~1.0×10-4 mol/L. The linear regression equation was y(mmol/ L ) =0.020 98x-0.020 59(related coefficient 0.993 5). Recovery experiments of standard addition in water had an average recovery of 97.2%. The detection limit was 1.0×10-7 mol/L. The relative standard deviation was 3.84%when the determination was conducted 5 times at 5.0×10-5mol/L.
【Fund】: 江苏省教育厅资助项目(JHZD04-010 02KJD15009)
【CateGory Index】: TP212.2
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