Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chemical Analysis and Meterage》 2009-03
Add to Favorite Get Latest Update

DETERMINATION OF TRACE STIBIUM CONTENT IN STEEL BY HYDRIDE GENERATION-ATOMIC FLUORESCENCE SPECTROMETRY

Yang Huiling1,Du Tianjun1,Tang Jing2,Han Huayun3,Zhang Xilin3 (1.General Institute for Nonferrous Metals and Explore for Mineral,Zhengzhou 450002,China;2.Institute of Antiquities and Archaeology,Zhengzhou 450000,China;3.Center of Analysis and Test,Zhengzhou University,Zhengzhou 450052,China)  
The determination of stibium in steel by hydride generation-atomic fluorescence spectrometry(HG-AFS) was developed.Interference effect of coexistent elements in steel such as Cu,V,Cr,Mn,Mo,Si,W,Ni and Ti on the determination of stibium was investigated.The influence of instrument parameters such as atomizer height,carrier gas rate,shield gas rate and concentration of HCl and KBH4 on the determination of stibium were studied and the conditions were optimized.The results showed that Kalium iodide and ascorbic acid were not only the best beforehand reducer for Sb5+,but also the occultation reagent for Fe,Cu,V,Cr,Mn,Mo,Si,W and Ti.Interference of Ni was eliminated by using EDTA-Thiourea.Under the optimized conditions,the linear range of stibium was 0-120 ng/mL,and the detection limit was 0.24 ng/mL.The relative standard deviation of determination result was 5.1%(n=10).Standard samples were determined by the method and the detection results were cosistent with the standard values.
【CateGory Index】: TG115.33
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【References】
Chinese Journal Full-text Database 3 Hits
1 MA Chong-xian,LI Sha-sha and WANG Yan(Center of Testing,Shanghai Research Institute of Materials,Shanghai 200437);Analysis of metallic materials[J];Chinese Journal of Analysis Laboratory;2011-02
2 Yang Huiling,Du Tianjun(General Institute for Nonferrous Metals and Explore fo Mineral,Zhengzhou 450002,China)Tang Jing(Institute of Antiquities and Archaeology,Zhengzhou 450000,China)Zhou Jie,Han Huayun(Center of Analysis and Test,Zhengzhou University,Zhengzhou 450052,China);DETERMINATION OF TRACE ARSENIC CONTENT IN STEEL BY HYDRIDE GENEATION-ATOMIC FLUORESCENCE SPECTROMETRY[J];Chemical Analysis and Meterage;2009-05
3 Zhao Yanbing,Liu Aikun,Dai Xueqian,Wang Jun (Technology Center,ShanXi Taigang Stainless Steel Co.Ltd.,Taiyuan 030003,China);Determination Progress of Trace Elements(Lead,Tin,Arsenic,Antimony,Bismuth)in Staliness Steel Alloys by HF-AFS[J];Modern Scientific Instruments;2011-03
【Citations】
Chinese Journal Full-text Database 10 Hits
1 SUN Xi Li YING Hai Song YU Qing (Beilun Import & Export Commodity Inspection Bureau,No.33 Mingzhou Lu,Beilun,Ningbo,Zhejiang 315800,P.R.China) CHEN Jian Guo (Ningbo Entry Exit Inspection & Quarantine Bureau,No.144 Liutingjie,Ningbo,Zhejia;Determination of Arsenic,Antimony and Bismuth in Iron Ore by FI-HG-AAS[J];CHINESE JOURNAL OF SPECTROSCOPY LABORATORY;2000-01
2 JIN Kui (Environment Science Department,Liaoning University,Shenyang 110036,P.R.China) GUO Xing-Jia TONG Jian JIANG Yu-Chun GUAN Hong-Yu (College of Chemistry Science and Engineering,Liaoning University,Shenyang 110036,P.R.China);Determination of Trace Element Sb in High Purity Nickel by GFAAS with STPF Technigue[J];Chinese Journal of Spectroscopy Laboratory;2003-03
3 GUO Xing-jia~(1,2),XU Shu-kun~(1*),LI Xiao-zhou~3,TONG Jian~2, SUN Ying~4,GUO Li-li~41.Chemistry Department of Northeast University,Shenyang 110004,China2.College of Chemistry Science and Engineering,Liaoning University,Shenyang 110036,China3.The Center of Photoelectron and Laser-Biomedical Research,Shenyang Ligong University,Shenyang 110168,China4.Institute of Metals,Chinese Academy of Sciences,Shenyang 110016,China;Determination of As,Pb,Sn,Sb and Bi in High Temperature Iron and Nickel-Based Alloy by Graphite Furnace Atomic Absorption Spectrometry Combined with Liquid-Liquid Extraction[J];Spectroscopy and Spectral Analysis;2006-06
4 Han Huayun, Liu Jia, Xu Yayun, Zhang Xilin (Department of Chemistry, Zhengzhou University, Zhengzhou 450052, China);DETERMINATION OF TRACE BISMUTH IN STEEL BY HYDRIDE GENERATION-ATOMIC FLUORESCENCE SPECTROMETRY[J];Chemical Analysis and Meterage;2007-05
5 Tang Lianxian (Jinhua Measurement and Test Institute for Quality and Technique Supervision, Jinhua 321000, China)Wu Xiao(Jinhua City CHELBI Engineering Consulting Co.ltd, Jinhua 321000, China)Zheng Shaocheng(Zhejiang Normal University, Jinhua 321000, China);DETERMINATION OF TRACE LEAD IN SPIRITS BY HYDRIDE GENERATION-ATOMIC FLUORESCENCE SPECTROMETRY[J];Chemical Analysis and Meterage;2008-02
6 WANG Zhao-zhong,FENG Xian-jin(Beijing General Research Institute of Mining and Metallurgy,Beijing 100044,China);HG-AFS DETERMINATION OF TRACE AMOUNTS OF ANTIMONY IN HIGH-PURITY LEAD[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2006-01
7 DAI Ya ming (Testing Centre of Materials for M achinery Industry,Shanghai 200437, China);Determination of arsenic,anti mony and bismuth in steel by hydride generation atomic absorption spectro scopy[J];Metallurgical Analysis;2001-06
8 NIE Ling-qing*1,JI Hong-ling1,CHEN Yin-yin1,LIU Xiao-ping1,WANG Yang-ping2(1.Technology Center of Baosteel Co.Ltd.,Shanghai 201900,China;2.University of Shanghai Science and Technology,Shanghai 200237,China);Determination of trace elements in steel by high resolution inductively coupled plasma mass spectrometry without matrix separation[J];Metallurgical Analysis;2007-02
9 CHEN An-ming(China South Rail Ziyang Locomotive Co.,Ltd.,Ziyang 641301,China);Determination of trace As,Sb,Bi,Sn and Pb in steel and pig iron by inductively coupled plasma-atomic emission spectrometry[J];Metallurgical Analysis;2007-03
10 HAN Hua-yun1,TANG Jing1,WANG Zhe-guang 2,ZHANG Xi-lin1(1.Department of Chemistry,Zhengzhou University,Henan 450052,China;2.College of Information and Management Science,Henan Agricultural University,Henan 450052,China);Determination of trace tin in steel by hydride generation atomic fluorescence spectrometry[J];Metallurgical Analysis;2008-06
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 YAO Zhen-xing,XIN Xiao-dong,SI Wei,ZHAO Jie,CHEN Guo-dong,ZHAO Wei,YANG Jian,DU Bin (School of Resources and Environmental Sciences,University of Jinan,Jinan 250022,China);Progress in Study on Detection of Heavy Metals[J];Analysis and Testing Technology and Instruments;2011-01
2 Ren Ping, Zhou Liyi (Institute of Geophysical & Geochemical Exploration, Langfang 065000);Determination of Lead in Vegetation and Human Hair Sample by Hydride Generation Atomic Fluorescence Spectrometry[J];Chinese Journal of Analytieal Chemistry;1998-04
3 Ren Ping (Institute of Geophsical & Geochemical Exploration,Langfang, Hebei, 065000);Determination of Lead in Geochemical Standard Materials by HG AFS Utilizing Alkaline Potassium Ferricyanide System[J];JOURNAL OF ANALYTICAL SCIENCE;1998-04
4 Guo Xiaowei and Guo Xuming (Northwest Research Institute of Geology, Xi'an 710054);Atomic Absorption, Atomic Fluorescence Spectrometry and Flame Emission Spectrometry[J];Analytical Laboratory;1993-04
5 Fan Jian(Instrument test and Analysis Centre,Central South University of Technology,Changsha,410083),Luo Chongqing(De-partment of Chemistry,Central South University of Technology,Changsha 410083),Fenxi shiganshi,1994,13(5),88-110This is the first biennial;Metallurgical Analysis[J];Analytical Laboratory;1994-05
6 LUO Li-qiang, MA Guang-zu and ZHAN Xiu-chun (National Research Center of Geoanalysis, Beijing, 100037);Geochemical analysis[J];Analytical Laboratory;2002-02
7 MA Chong-xian~* and WU Cheng(Shanghai Research Institute of Materials,Shanghai 200437);Analysis of metallic materials[J];Chinese Journal of Analysis Laboratory;2006-12
8 SHU Yong-hong1,2 and He Hua-kun*1(1.Chinese National Analytical Center,Guangzhou 510070,2 Guangdong Key Laboratory of Chemical Emergency Test),Fenxi Shiyanshi,2007,26(8): 106~122;Atomic absorption spectrometry and atomic fluorescence spectrometry[J];Chinese Journal of Analysis Laboratory;2007-08
9 WEI Bi-wen1, MIAO Jun-wen1, ZHANG Ning1, GONG Zhi-xiang2 and ZHANG Hong-liang2 (1. Shanghai Entry-Exit Inspection and Quarantine Bureau, Shanghai 200135; 2. Department of Applied Chemistry, East China Institute of Technology, Linchuan 344000);Determination of trace arsenic and antimony in textiles by miniature hydride generation atomic absorption spectrometry[J];Chinese Journal of Analysis Laboratory;2009-03
10 ZANG Mu-wen and LIU Chun-xiao(General Research Institute for Nonferrous Metals,Beijing 100088);Analysis of metallic materials(Ⅰ)[J];Chinese Journal of Analysis Laboratory;2009-04
China Proceedings of conference Full-text Database 4 Hits
1 NIE Lingqing (Technology center of baosteel Co. Ltd., Shanghai 201900, China);Determination of Trace Elements Ce in Low Alloy Steel by High Inductively Coupled Plasma Mass Sepctrometry[A];[C];2008
2 SHAN Hai-xia and LI Zai-jun College of Chemical and Material Engineering, Southern Yangtze University, Wuxi 214036, China;A novel Room Temperature Ionic Liquid 1-Butyl-3-trimethylsilylimidazolium hexafluorophosphate as Solvent for Preconcentration of trace Lead in Dialysis Fluids and its Determination by Graphite Furnace Atomic Absorption Spectrometry[A];[C];2006
3 SHEN Zhiyun LI Shasha MA Chongxian Testing Center, Shanghai Research Institute of Materials, Shanghai 200437;HYDRIDE GENERATION-ATOMIC FLUORESCENCE SPECTROMETRY & RECENT PROGRESSES ON ITS APPLICATION FOR DETERMINATION OF TRACE AMOUNT OF ELEMENTS IN METAL MATERIALS[A];[C];2008
4 Xiangrong XIANG,Hong LIU,Jiao WANG Chongqing Instrument Materials Research Institute,Chongqing,China,400700;Determination of Trace of Bismuth in High Temperature Alloys by Hydride Generation-Atomic Fluorescence Spectrometry[A];[C];2011
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 SUN Shu-jing (Liaozhong Water-conservancy chemical Engineering Works,Liaozhong,Liaoning 110200,China);Rapid Determination of Magnesium in Aluminum Alloys[J];Sichuan Nonferrous Metals;2007-03
2 HE Yong(Guangdong Test Center of Product Quality Supervision,Shunde 528300);Determination of Silver,Copper,Lead Content in Lead-free Soldering Tin by ICP-AES[J];Sichuan Nonferrous Metals;2008-03
3 WANG Xue-jing(Sichuan Research Institute of Non-ferrous metals Metallurgy,Chengdu 610081,Sichuan,China);Fast Determinating of low content tin in silicon-aluminum alloy[J];Sichuan Nonferrous Metals;2009-01
4 He Yong(Guangdong Test Center of Product Quality Supervision,Shunde 528300);Microwave digestion MICP-AES tests main alloying elements in Cr12 high carbon steel[J];Sichuan Nonferrous Metals;2009-01
5 HE Yan-ming,LIU Zi-ping,WANG Shan-fei,LEI Li(Center Laboratory Of Sichuan Aostar Aluminium Company With Limited Liability,Sichuan Meishan 620041);Capacity Determination of Boron in Aluminum Alloy[J];Sichuan Nonferrous Metals;2009-02
6 WU Shui-ying(Xiamen Municipal Construction Science Research Institute,Xiamen 361004,China);Determination of Cerium in Akaline Zn-Ce Alloy Plating Bath by Colour-Fading Spectrophotometry[J];Electroplating & Pollution Control;2009-04
7 Qiu Deren (Department of Chemistry);REACTION MODES OF STANNANE GENERATION[J];Journal of Fudan University(Natural Science);1992-01
8 Chen Xiangming Wan Danhong Jiang Hui(Inspection and Quarantine Technical Centre, Fujian Entry-exit Inspection and Quarantine Bureau,Fuzhou,Fujian 350001,China);Study on the effects of various reducers on determination of arsenic in foodstuff[J];Fujian Analysis & Testing;2007-02
9 Huang Yunhua(The Quality and Metrology Department of Sanming Iron & Steel Co.LTD,Sanming,365000,China);Determination of Phosphorus in Silicomanganese and Ferromanganese Alloys by ICP-OES[J];Fujian Analysis & Testing;2008-02
10 Huang Yun-hua(The Quality and Metrology Department of Sanming Iron & Steel Co.,LTD of Fujian,Sanming,Fujian 365000,China);Study on the repeated use of the porcelain crucible and joining amount of flux by Instrument of high-frequency infrared of carbon and Sulphur[J];Fujian Analysis & Testing;2009-02
【Secondary References】
Chinese Journal Full-text Database 2 Hits
1 TANG Zhi-yong,QIU Hai-ou and ZHENG Hong-tao (Faculty of Material and Chemistry,China University of Geosciences,Wuhan 430074);Progress in atomic emission spectrochemical analysis[J];Chinese Journal of Analysis Laboratory;2011-12
2 Zhao Yanbing,Liu Aikun,Dai Xueqian,Wang Jun (Technology Center,ShanXi Taigang Stainless Steel Co.Ltd.,Taiyuan 030003,China);Determination Progress of Trace Elements(Lead,Tin,Arsenic,Antimony,Bismuth)in Staliness Steel Alloys by HF-AFS[J];Modern Scientific Instruments;2011-03
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 FENG Dongwen GUO Yu LIU Jianchun(State Key Laboratory for Powder Metallurgy, Central South University, Changsha 410083, China);Determination of tin in the iron, steel and alloy by carrying settle and phenylfluorone-CTMAB photometric[J];Materials Science and Engineering of Powder Metallargy;2002-02
2 Wang Xiu Fang Zhaolun (Institute of Forestry and Soil Science,Academia Sinica,Shenyang);A SEMI-AUTOMATED FLOW INJECTION ANALYSIS SYSTEM FOR THE DETERMINATION OF TRACE ARSENIC BY HYDRIDE GENERATION ATOMIC ABSORPTION SPECTROMETRY[J];Chinese Journal of Analytical Chemistry;1988-10
3 Xie Wenbing; YaoJinyu; Hu Qinglan; Meng Xiumei; LianChengzhang(Changchun Institute of Ap-plied Chemistry,Chinese Academy of Sci-ences,Changchun 130022);Direct Determination of Bismuth in High Temperature Nickel-based Alloy byPlatform Graphite Furnace Atomic Ab-sorption Spectrometry[J];ANALYTICAL LABORATORY;1995-02
4 SUN Xi Li YING Hai Song YU Qing (Beilun Import & Export Commodity Inspection Bureau,No.33 Mingzhou Lu,Beilun,Ningbo,Zhejiang 315800,P.R.China) CHEN Jian Guo (Ningbo Entry Exit Inspection & Quarantine Bureau,No.144 Liutingjie,Ningbo,Zhejia;Determination of Arsenic,Antimony and Bismuth in Iron Ore by FI-HG-AAS[J];CHINESE JOURNAL OF SPECTROSCOPY LABORATORY;2000-01
5 FANG Hong YANG Xiao\|Bing (Shanxi Entry\|Exit Inspection and Quarantine Bureau,No.20 Yifenjie,Taiyuan 030024,P.R.China);Determination of As,Pb and Hg in Cosmetics by Inductively Coupled Plasma Atomic Emission Spectrometry[J];Chinese Journal of Spectroscopy Laboratory;2002-01
6 LI Hai-Ming YANG Shao-Bina (The Synthetical Group of Chaidamu Geological Survey,Germ,Qinghai 816000,P.R.China) a(Tianjin Institute of Urban Construction,Tianjin 300384,P.R.China);Determination of Sn in Iron Ore by Hydride Generation-Atomic Fluorescence Spectrometry[J];Chinese Journal of Spectroscopy Laboratory;2005-02
7 Qingbin LIU Central Iron and Steel Research Institute,100081 Beijing;Determination of Trace Bismuth in Iron, Steel and Alloy by Hydride Generation Atomic Fluorimetry[J];SPECTROSCOPY AND SPECTRAL ANALYSIS;2000-01
8 GUO Xing jia 1, JING Kui 1, JING Run 1, YANG Qi 1, LIU Xin 2 and TANG Xia 2 1. College of Chemistry Science and Engineering, Liaoning University, Shenyang 110036, China 2. Shenyang Liming Motor Group, Shenyang 110043, China;Direct Determination of Trace Element Arsenic in High Purity Nickel by GFAAS[J];Spectroscopy and Spectral Analysis;2002-06
9 GUO Xing-jia~(1,2),XU Shu-kun~(1*),LI Xiao-zhou~3,TONG Jian~2, SUN Ying~4,GUO Li-li~41.Chemistry Department of Northeast University,Shenyang 110004,China2.College of Chemistry Science and Engineering,Liaoning University,Shenyang 110036,China3.The Center of Photoelectron and Laser-Biomedical Research,Shenyang Ligong University,Shenyang 110168,China4.Institute of Metals,Chinese Academy of Sciences,Shenyang 110016,China;Determination of As,Pb,Sn,Sb and Bi in High Temperature Iron and Nickel-Based Alloy by Graphite Furnace Atomic Absorption Spectrometry Combined with Liquid-Liquid Extraction[J];Spectroscopy and Spectral Analysis;2006-06
10 HUO Guangjin,YAN Junying and WANG JiafengDepartment of Chemistry,Hebei Teacher′s College,050091 Shijiazhuang;DETERMINATION OF TRACE COPPER AND LEAD IN HIGHLY PURE SAMARIA BY EXTRACTIONGRAPHITE FURNACE ATOMIC ABSORPTION SPECTROMETRY[J];SPECTROSCOPY AND SPECTRAL ANALYSIS;1998-01
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved