Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Chemical Reaction Engineering and Technology》 2004-02
Add to Favorite Get Latest Update

Synthesis of Nipagin Esters Catalyzed by Vitamin C

Xu Wenyuan Ma Jianguo Peng Daofeng (Department of Applied Chemistry, East China Institute of Technology, Fuzhou 344000, China)  
Nipagin esters was synthesized by the esterification of n-butyl and iso-butyl alcohol with p-hydroxybenzoic acid in the presence of vitamin C. The effect of acid and alcohol mole ratio, the amount of vitamin C catalyst and reaction time on the yield of Nipagin esters was investigated. Under optimal conditions, the yield of n-butyl p-hydroxybenzoate was 93. 3% and the yield of iso-butyl p-hydroxybenzoate was 91. 3%. The results indicated that vitamin C possessed a fairly high catalytic activity for the esterification reaction.
【CateGory Index】: TQ245
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
Chinese Journal Full-text Database 10 Hits
1 Xie Jianying,Huang Fu(College of Science,Guangdong Ocean University,Zhanjiang 524088,China);Synthesis of Benzaldehyde Ethylene Glycol Acetal under Microwave Irradiation Catalyzed by Vitamin C[J];Guangdong Chemical Industry;2013-02
2 Yao Xiaoqing;Tang Yong;Gong Yujun;Chemistry and Life Science College,Guang Dong University of Petrochemical Technology;Department of Experiment Teaching,Guang Dong University of Petrochemical Technology;;Study on the Process and Corrosion Performance of Silicotungstic Acid Catalytic Synthesis of Ppreservative Nipagin Ester[J];Guangdong Chemical Industry;2014-03
3 SUN Ting,LI Jing,ZHENG Rui-fang,HUANG Xiao-dong(College of Chemistry and Engineering,Xuchang University,Xuchang 461000,China);Synthesis of Cyclohexyl Acetate Catalyzed by Vitamin C[J];Journal of Hubei University for Nationalities(Natural Science Edition);2009-02
4 Ma Changai Wei Yan Li Fanghang(Department of Chemistry,Guangxi Nanning Prefecture Education College,Guangxi Nanning 530001);Catalytic Synthesis of Butyl p-Hydroxybenzoate with SnCl_4·5H_2O under Microwave Irradiation[J];Chemical Industry Times;2005-10
5 SHAO Gui-zhen1,HE Jian-ying2,CHEN Dan-yun2(1.Kaifeng Pharmaceutical Group Corporation,Kaifeng 475003,China;2.Chemistry and Chemical Engineering College of Henan University,Kaifeng 475004,China);Catalytic Synthesis of Isobutyl P-hydroxybenzoate[J];Hebei Chemical Engineering and Industry;2010-06
6 LIU Mei-yan, YU Shan-xin, GUAN Shi-bin (College of Chemistry and Chemical Engineering,Hunan Normal University,Changsha 410081,China);Research Progress in Catalysts for Synthesizing p-Hydroxyl Butyl Benzoate[J];Chemical Propellants & Polymeric Materials;2006-04
7 JIN Lie,LIN Pei-xi(College of Chemistry and Life Science,Guangdong University of Petrochemical Technology,Maoming 525000,China);Dibutyl Oxalate Synthesized from Vitamin C[J];Journal of Guangdong University of Petrochemical Technology;2011-01
8 WANG Shu-li1,ZHANG Xia2,HE Jian-ying1,ZHANG Fu-lian1,CHEN Dan-yun1(1.College of Chemistry and Chemical Engineering,Henan University,Kaifeng 475004,China;2.College of Continuous Education,Zhengzhou University of Light Industry,Zhengzhou 450002,China);Synthesis of isobutyl p-hydroxybenzoate catalyzed by gallium sulfate[J];Applied Chemical Industry;2009-10
9 HU Yu-yuan;ZHANG Ya-dong;School of Chemical and Energy,Zhengzhou University;;Efficient synthesis of n-butyl-p-hydroxybenzoate preservative with toluene-4-sulfonic acid as catalyst[J];Applied Chemical Industry;2014-07
10 LIU Yu-ting,CHEN Xu,YIN Da-wei,LV Bo(School of Chemistry and Chemical Engineering,Shaanxi University of Science & Technology,Xi'an 710021,China);Research development on the synthesis of paraben[J];China Condiment;2009-08
Chinese Journal Full-text Database 4 Hits
1 LONG Li ping 1, ZHONG Tong sheng 1, WEN Rui ming 1, YU Shan xin 1,2 (1. Department of Chemistry, Yiyang Teacher's College, Yiyang 413049, China;(2. College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081,;Synthesis of Isobutyl p Hydroxybenzoate Catalyzed by Sodium Bisulfate[J];Chinese Journal of Synthetic Chemistry;2002-01
2 DING Liang-zhong, YU Shan-xin, WEN Rui-ming, LUO Xin-xiang (Department of Chemistry,Hunan City College,Yiyang 413049, Chian);Catalytic Synthesis of n-Butyl Lactae with Vitamin C[J];Chinese Journal of Synthetic Chemistry;2002-03
3 ;硫酸氢钠催化合成尼泊金丁酯[J];Science and Technology of Food Industry;2003-03
4 ;A new-type food preservative-Nipagin[J];Chinese Condiment;2003-03
Chinese Journal Full-text Database 10 Hits
1 WANG Xue-mei,HUANG Hong,WU Mi-mi,LIU Jun-liang(College of Chemistry and Chemical Engineering,Anhui University,Hefei 230039,China);The preparetion and identification of inclusion compounds of β-cyclodextrin with propylparaben[J];Journal of Anhui University(Natural Sciences);2008-06
2 WANG Xue-mei,WU Mi-mi,HUANG Hong,QIN Da-quan(College of Chemistry and Chemical Engineering,Anhui University,Hefei 230039,China);Study on solutions of inclusion compounds of β-cyclodextrin with propylparaben by spectra[J];Journal of Anhui University(Natural Sciences Edition);2010-02
3 Zhou hongping(Departmentofchemistry,Anhuiuniversity,Hefei 230039);Application of the Nonliquid Catalyst in Ester Reaction[J];Anhui Chemical Industry;2002-03
4 YU SHan-xin 1 WEN Rui-ming 2 LONG Li-ping 1 (1.Department of Chemistry and Chemical engineering, Hunan Normal University,Changsha Hunan,410081) (2.Department of Chemistry,Hunan Urban College, Hunan Yiyang 413049);CATALYTIC SYNTHESIS OF n-BUTYL LACTATE WITH SOLID ACID[J];Journal of Changde Teachers University;2003-01
5 YU Shan-xin~1,WEN Rui-ming~2,LI Wang-ying~2 (1.College of Chemistry and Chemical Engineering,Hunan Normal University,Changsha410081,China; 2.Department of Chemistry and Environmentally Engineering,Hunan City University,Yiyang413049,China);Synthesis of isobutyl p-hydroxybenzoate catalyzed by amino sulfonic acid[J];China Surfactant Detergent & Cosmetics;2003-06
6 WANG Xiao-long,SUN Jun-yong (College of Chemistry and Material Science,Anhui Normal University,241000,Wuhu,Anhui,China);Study on Synthesis of Sodium Methylparaben[J];Journal of Huaibei Coal Industry Teachers College(Natural Science Edition);2009-03
7 GAO Wen-yi,REN Li-guo,ZHANG Xiao-li(School of Petrochemical Technology,Liaoning University of Petroleum & Chemical Technology,Fushun Liaoning 113001,P.R.China);Catalytic Synthesis of Ethyl p-Hydroxybenzoate With the Solid Superacid S_2O_8~(2-)/ZrO_2-Al_2O_3[J];Journal of Liaoning University of Petroleum & Chemical Technology;2006-03
8 ;The antisepsis effect of nipagin ethyl ester to Bombyx mori artificial diet to experiment[J];Guangxi Sericulture;2010-02
9 LI Fang liang, WEI Qun lan, LI Yue zhen (Department of Chemistry, Guangxi Nanning Prefecture Education College, Nanning 530001,China);Rapid Synthesis of Butyl p-Hydroxybenzoate[J];Guangxi Chemical Industry;2002-02
10 Li Fangliang Li Yuezhen Wei Hanchang(Department of Chemistry,Nanning Prefecture Education College,Beihulu,Nanning,Guangxi,530001,China);Synthesis Conditions of Butyl Oleate under Microwave Field[J];Guangxi Sciences;2002-04
China Proceedings of conference Full-text Database 1 Hits
1 HE Yin-ju,YANG Zai-bo,MAO Hai-li,LIU Kang-lian Department of Chemistry,Qiannan Normal University for Nationalities,Duyun 558000,China;The Recent Progress in the Application of the Microwave Technique in Modern Organic Synthetic Chemistry[A];[C];2013
Chinese Journal Full-text Database 10 Hits
1 WANG Jun-feng,LI Zi-rong(Department of Applied Chemistry,Anhui Science and Technology University,Fengyang 233100,China);Research of the Bacteriostatic Effects of Cosmetic Antiseptic of Nipagin Ester[J];Journal of Anhui Science and Technology University;2008-04
2 Lin Shijing (Department of Chemical Engineering , Beijing Institute of Petro-chemical Technology, Beijing 102617) Sun Yangzhao (Research Center for Eco-environmental Science , Chinese Academy of Sciences, Beijing 100085);Summarization of Synthetic Methods of Food Preservatives[J];Journal of Beijing Institufe of Petrochemical Technology;2004-03
3 XU Jing-shi, CHEN Hui-zong (Institute of Chemistry and Biological Science,Jiangxi Normal Universit y,Nanchang 330027,China);The Study of Rare Earth Solid Superacids for Catalytic Synthesis of Hydroxybenzoic Ethers[J];JOURNAL OF JIANGXI NORMAL UNIVERSITY (NATURAL SCIENCES EDITION);2000-02
4 XU Jing Shi, ZHOU Guo Bin, WANG Hong Ming, CHEN Hui Zong (Institute of Chemistry and Biology Sciences,Jiangxi Normal University,Nanchang 330027,China);Study on Synthesis of Hydroxybenzoic Esters with TiO_2/SO_4~(2-) Solid Acids Zeolites as Catalyst[J];Journal of Jiangxi Normal University (Natural Sciences Edition);2002-01
5 Shi Xiaobo Li Chungen (Department of Chemistry,Jiangxi Normal University,Nanchang 330027);Synthesis of Butyl p Hydroxybenzoate with Dodecatungstophosphoric Acid Catalyst[J];JOURNAL OF JIANGXI NORMAL UNIVERSITY (NATURAL SCIENCES EDITION);1998-04
6 LI Xiao li BAI Xiu li WANG Xiao ju (Department of Chemistry, Changchun Teacher's College, Changchun 130032, China);Preparation of Nipagin Esters with Catalyst Solid Nd 2O 3[J];JOURNAL OF CHANGCHUN TEACHERS COLLEGE;1999-05
7 YU Shan-xin1, FANG zheng-fa1, WEN Rui-ming2 (1.College of Chemistry and Chemical Engineering,Hunan Normal University, Changsha Hunan, 410081; 2. Department of Chemistry and Environmentally Engineering, Hunan City University, Yiyang Hunan, 413049);Synthesis of n-Butyl p-Hydroxy Benzoate Catalyzed by Amino Sulfonic Acid[J];;2005-02
8 ;甲壳质负载四氯化锡催化合成对羟基苯甲酸丁酯[J];Journal of Hebei Tourism Vocational College;2008-02
9 YANG Shui-jin~1 LIANG Yong-guang~1 YU Xin-wu~1 SUN Ju-tang~2 [WT4”BZ](1.Department of Chemistry,Hubei Normal University, Huangshi 435002,China 2.Department of Chemistry,Wuhan University, Wuhan 430072,China);Catalytic Synthesis Nipagin Esters with TiSiW_12O_40/TiO_2[J];China Surfactant Detergent & Cosmetics;2000-04
10 FENG Wu wen,YANG Cun,YU Hong qi(Xinte Science & Technology Development Co. Ltd., Beijing University of Chemica l Technology,Beijing 100029,China);Molecular distillation technology and daily-use chemical industry (Ⅰ) the principle and characteristics of molecular distillation[J];China Surfactant Detergent & Cosmetics;2002-05
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 PATIMA Nizamidin,ABLIZ Yimit(College of Chemistry and Chemical Engineering,Xinjiang University,Urumqi 830046);PVA THIN FILM BASED OPTICAL WAVEGUIDE SENSOR AND ITS APPLICATION IN XYLENE DETECTION[J];Acta Polymerica Sinica;2011-04
2 LIU Xiao-lin (Department of Chemistry, Jiaying University, Meizhou 514015, China);Synthesis of Butyl p-Hydroxybenzoate with Sulfates as Catalysts[J];Guangzhou Chemical Industry;2007-04
3 Xie Jianying,Huang Fu(College of Science,Guangdong Ocean University,Zhanjiang 524088,China);Synthesis of Benzaldehyde Ethylene Glycol Acetal under Microwave Irradiation Catalyzed by Vitamin C[J];Guangdong Chemical Industry;2013-02
4 Hao Hongying;Zhou Fang;Zhang Qiang;Li Hailing;Zhang Shasha;Medical School,HuangHe Science and Technology College;;Synthesis of Acetylsalicylic Acid under Microwave Radiation Condition by Vitamin C[J];Guangdong Chemical Industry;2013-17
5 Gao Danping;Cai Yu;Mei Laibao;College of Sciences, Nanjing University of Technology;;Synthesis of Butyl Paraben Catalyzed by Solid Super Acid La~(3+)-SO_4~(2-)/TiO_2-Fe_2O_3[J];Guangdong Chemical Industry;2013-20
6 Li Jinghua, Li Zhenqiu, Yu Guang, Zhang Yuanjing, Huang Caixia (College of Chemical Engineering, Qingdao University of Science & Technology, Qingdao, Shandong 266042);The Green Process of Preparing Rubber Accelerator CBS without Solvent[J];Chemical Production and Technology;2009-06
7 Yu Shanxin, Liu Meiyan, Zhu Ailing (College of Chemistry and Chemical Engineering Hunan Normal University Chang sha 410081);Research Progress in Catalysts for Synthesis of p-hydroxyl n-propyl Benzoate[J];China Chemicals;2008-04
8 ZENG Li-hua,LIU Li-min,LUO Jian-li,YIN Du-lin(School of Chemistry & Chemical Engineering,Hunan Normal Univeisity,Changsha,Hunan 410081,China);Study on the Synthesis of Butyl p-Hydroxybenzoate[J];Journal of Hunan City University(Natural Science);2007-04
9 ZENG Li-hua,LI Qi-hua,LEI Chun-hua,YIN Du-lin(Colloge of Chemistry and Chemical Engineering,Hunan Normal Univeisity,Changsha 410081,China);Synthesis of Parabens Catalyzed by Sulfoacid Resin[J];Fine Chemical Intermediates;2007-06
10 Qian Yunhua Jin Yeling Chen Jing Hu Tao Tan Liqiang Wang Jie (Chemical Engineering Department, Huaiyin Institute of Technology,Huaian 223003, Jiansu, China);SYNTHESIS OF BUTYLPARABEN WITH SOLID SUPERACID SO_4~(2-)/TiO_2 ATTAPULGITE AS CATALYST[J];Speciality Petrochemicals;2008-01
【Secondary Citations】
Chinese Journal Full-text Database 6 Hits
1 Cheng, Ben-cheng; Liu, Yong; Hong, Yong;and Yi, Lun(Department ot Chereistfg, Central South Universitg of Technologg, Changsha 410083);ESTERIFICATION OF SUBSTITUTED BENZOIC ACIDS WITH n-BUTANOL CATALYZED BY SOLID CATALYSTS[J];CHINESE JOURNAL OF CATAL YSIS;1994-01
2 YU Shan-xin 1, LI Wang-ying 2, XIONG Wen-gao 2 (1.Hunan Normal university, Changsha 410008 ,China ; 2.Yiyang Teacher's College, Yiyang , 413049,China);Catalytic synthesis of n-butyl lactate with sodium bisulfate[J];Journal of Hubei Institute For Nationalities;2001-01
3 Zeng Hanwei', Li Kunzhi, Zheng Huajun, LuoRe (Department of Applied Chemistry, South ChinaUniversity of Technology, Guangzhou 510641 );Improved synthetic method for p-hydroxybenzoic esters[J];CHEMICAL REAGENTS;1996-06
4 Yang Shuijin (Department of Chemistry,Hubei Normal University,Huangshi 435002 );Synthesis of Butyl Lactate[J];Shaanxi Chemical Industry;1999-04
5 Lin Shen,Yan Guiyang,Xu Limin,Peng Yiru and Zhuang Naifeng (Department of Chemistry,Fujian Normal University,Fuzhou 350007);Synthesis of p Hydroxybenzoate Catalyzed by Phosphato Tungstic Acid[J];PETROCHEMICAL TECHNOLOGY;1998-09
6 Lei Cunxi\ Wen Ruiming\ Yu Shanxin (Chemistry Department,Yiyang Teacher's College,Yiyany,Hunan\ 413049);The Study of Catalytic Synthesis of Acetic Esters with Sodium Bisulfate[J];Journal of Xingjiang Normal University(Natural Sciences Edition);2001-01
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved