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《Chemical Reagents》 2004-05
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Study on synthesis of 2-propene-1-thiol

LIU Yu-ping~*,SUN Bao-guo,XIE Jian-chun,ZHENG Fu-ping,XIAO Yang (School of Chemical and Environmental Engineering,Beijing Technology and Business University,Beijing 100037)  
Propene-1-thiol was prepared by hydrolyzing S-allyl-iso-thiourea bromide in aqueous solution of sodium hydroxide and acidifying with dilute sulfuric acid.S-Allyl-iso-thiourea bromide could be synthesized by the reaction of allyl bromide with thiourea in aqueous solution of tetrabutyl ammonium bromide.The content and structure of 2-propene-1-thiol were confirmed by GC and IR.
【CateGory Index】: TQ655
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