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《Chemical Reagents》 2008-02
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Synthesis and structure of mixed dialkyl tin dichlorides

LIN Sen,XU Song,DENG Rui-hong,JIA Lu-lu (Department of Chemistry,Nanchang University,Nanchang 330031,China)  
Three mixed dialkly tin dichlorides have been synthesized by the reaction of tetralkyl tin with concentrated hydrochloric acid.Their structures were characterized by 1HNMR,13CNMR,and IR spectroscopy.The effects of temperature,molar ratio of reactants,and reaction time on product yield were investigated.The experimental results showed that the method had the advantage of simple operation,quick reaction,reduced pollution,and high yield to meet the demands of green chemistry compared with other methods.
【Fund】: 江西省自然科学基金资助课题(0520064);; 江西省教育厅基础研究资助项目(200650)
【CateGory Index】: O627.4
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