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《Chemical Reagents》 2008-03
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Study on the preparation of monolithic imprinted HPLC column

ZUO Guo-qiang1,ZHANG Yu-ping2,GONG Wen-jun2,ZHANG Yi-jun2,LI Quan-min1 (1.Department of Chemistry,Henan Normal University,Xinxiang 450007,China;2.Henan Institute of Science and Technology,Xinxiang 453003,China)  
A monolithic molecularly imprinted polymer with specific recognition ability for 4-hydroxybenzoic acid (4-HBA) was prepared by in-situ thermal polymerization,using acrylamide as the functional monomer,ethylene glycol dimethacrylate (EDMA) as the cross-linking agent,toluene and dodecanol as porogenic solvents and azobisisobutyronitrile (AIBN) as the thermal polymerization initiator.Baseline separation of isomers of hydroxybenzoic acid was achieved on the prepared HPLC imprinted column,but not on the blank polymer.The basic principle and mechanism of molecular imprinting polymers were discussed in this paper.
【Key Words】： molecularly imprinted polymer monolithic column high performance liquid chromatography
【Fund】： 中韩国际合作协议项目(20611140646);; 河南省高校新世纪优秀人才项目(2006HNCET-01)资助
【CateGory Index】： O657.7
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【References】
Chinese Journal Full-text Database 1 Hits
1 Jun-Xia Zhang 1,2, Na Chen 2, Sheng-Kai Yang 2, Zhan-Jun Yang 2, Yu-Ping Zhang 2* (1. Henan Provincial Institute of Food and Drug Control, Zhengzhou 450003, China; 2. Henan Institute of Science and Technology, Xinxiang 453003, China );Preparation and Evaluation of Methacrylate-based Monolithic Column for Capillary Liquid Chromatography[J];Life Science Instruments;2009-07
【Citations】
Chinese Journal Full-text Database 3 Hits
1 YANG Min-Li,LI Yuan-Zong * [WT5”BX](Key Laboratory of Bioorganic Chemistry & Molecular Engineering of Ministry of Education,College of Chemistry and Molecular Engineering,Peking University,Beijng 100871,China) [WT5HZ];Molecular Imprinting Mechanism Study with Benzoic Acid and Ethyl Benzoate Analogues as Templates[J];Chemical Research In Chinese Universities;2004-06
2 ZHANG Yu-Ping1,ZUO Guo-Qiang2,XU Guang-Ri1,LI Quan-Min2,YUAN Zhuo-Bin1,3(1. Institute of Applied Chemistry,Henan Institute of Science and Technology,Xinxiang 453003,China;2. Department of Chemistry,Henan Normal University,Xinxiang 453007,China; 3. Graduate School,Chinese Academy of Sciences,Beijing 100039,China);Rapid Preparation of Molecularly Imprinted Capillary Monolithic Columns by Microwave Polymerization[J];Chemical Journal of Chinese Universities;2007-09
3 ZHANG Jie 1,WANG Yong-jian *2 ,YU Ao 1 (1.College of Chemistry,Nankai University,Tianjin 300071,China;2.Key Laboratory of Bioactive Materials,Ministry of Education,Nankai University,Tianjin 300071,China);The application of molecular imprinting technique in steroid recognition and analysis[J];Chemical Reagents;2005-06
【Co-citations】
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1 LIU Qing-Hui,L Jiu-Ru~*,FENG Na(College of Chemistry and Material Science,Shaanxi Normal University,Xi′an 710062,China);Post Chemiluminescence Reaction of Dipyridamole in Luminol-potassium Ferricyanide System and Its Application in Analysis——The Molecular Imprinting-post Chemiluminescence Method for the Determination of Dipyridamole[J];Chemical Journal of Chinese Universities;2006-06
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3 ZHANG Yu-Ping1,ZUO Guo-Qiang2,XU Guang-Ri1,LI Quan-Min2,YUAN Zhuo-Bin1,3(1. Institute of Applied Chemistry,Henan Institute of Science and Technology,Xinxiang 453003,China;2. Department of Chemistry,Henan Normal University,Xinxiang 453007,China; 3. Graduate School,Chinese Academy of Sciences,Beijing 100039,China);Rapid Preparation of Molecularly Imprinted Capillary Monolithic Columns by Microwave Polymerization[J];Chemical Journal of Chinese Universities;2007-09
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6 LAN Li-xin(Hunan Chemical Industry Vocation Technology Institute,Zhuzhou,Hunan 412004,China);Study of molecularly imprinting technology and its application[J];Technological Development of Enterprise;2004-11
7 ZHANG Guo-sheng,DONG Xue-zhi,LI Chang,WANG Ai-fang (Pollution Control Institute, College of Chemistry and Chemical Engineering, Henan University, Kaifeng 475001, China);Evelopment of Determination Technique of Hormone Residues in Meat Products[J];Food Science;2008-02
8 ZHANG Cheng-li1,ZHOU Yan-mei1,MA Tong-sen1,LI Li-qing2(1.College of Chemistry and Chemical Engineering,Henan University,Kaifeng,475004;2.Department of Chemistry and Environmental Science,Taishan University,Tai'an,271021,China);Study and Application of Molecular Imprinting Technique in Pharmaceutical Analysis[J];Journal of Taishan University;2008-06
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【Co-references】
Chinese Journal Full-text Database 1 Hits
1 ZHANG Yu-Ping1,ZUO Guo-Qiang2,XU Guang-Ri1,LI Quan-Min2,YUAN Zhuo-Bin1,3(1. Institute of Applied Chemistry,Henan Institute of Science and Technology,Xinxiang 453003,China;2. Department of Chemistry,Henan Normal University,Xinxiang 453007,China; 3. Graduate School,Chinese Academy of Sciences,Beijing 100039,China);Rapid Preparation of Molecularly Imprinted Capillary Monolithic Columns by Microwave Polymerization[J];Chemical Journal of Chinese Universities;2007-09
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