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《Huaxue Shijie (Chemical World)》 2001-06
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Synthesis and Application of High Purity Etherizing Agent

JIAN Xiu jun DING Wen guang WAN Yong xiang AN Feng fa (Research Institute of Qilu Petrochemical Corporation Shandong Zibo 255400, China)  
Chloro 2 hydroxypropyl trimethyl ammonium chloride an etherizing agent,for modified starch, was synthesised from epichlorohydrin. The kind and quantity of catalyst and reaction time, which influence the yield of etherizing agent were investigated. The production condition were as follows: using quaternary ammonium catalyst, reaction time was 3 h, n (epichlorohydrin): n (trimethylamine salt)= 1.00:1.05, etherizing agent yield was above 98 %. In the product, epichlorohydrin (quality fraction)≤5×10 -6 , 1, 3 dichloropropanol(quality fraction)≤1×10 -5 . This etherizing agent is a goods detergent and a fragrant retention agent.
【CateGory Index】: TQ421
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