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《Huaxue Shijie (Chemical World)》 2001-09
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Synthesis of 3-Methylamino-1,2-propandiol

XIE Min-hao, LUO Shi-neng, HE Yong-jun, LIU Ya-lin, ZHOU Pei (Jiangsu Institute of Nuclear Medicine, State Key Laboratory of Nuclear Medicine, Jiangsu Wuxi 214063, China)  
Methylamino-1,2-propandiol is an important raw material of Iopromide. Its synthesis was from epichlorohydrin by hydrolysis and ammoniaiton. The overall yield was 41.3%. The results showed the best yield was 56.3% when the reaction temperature was 80℃ and the molar ratio of methylamine /3-chloro-1,2-propandiol was 4.5.
【CateGory Index】: TQ421.7
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