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《Huaxue Shijie (Chemical World)》 2004-07
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Preparation and Characterization of Heteropoly Acid Supported on Montmorillonite Modified by Surfactant Catalyst

ZHANG Cui-xian~1,TU Hua-min~(1*),LUAN Wen-lou~2 (1. Institute of Chemistry, Hebei Normal University, Hebei Shijiazhuang 050091, China; 2. Institute of Resources and Environmental Engineering, Shijiazhuang Economic Institute, Hebei Shijiazhuang 050016, China; 3. School of Chemistry and Chemical Engineering, Zhoushan University, Guangdong Guangzhou 510275, China)  
The heteropoly acid (PW_(12)) supported on montmorillonite modified by surfactant catalyst was prepared by means of impregnation and refluxing-adsorption methods. IR, XRD and DTA measurements showed that PW_(12) was well dispersed. The interaction between PW_(12) and montmorillonite modified by surfaction was enhanced. The catalytic activity, selectivity and stability of the catalyst for esterification were investigated. The results show that the refluxing-adsorption method is advantageous to prepare the catalyst.
【Fund】: 河北省科委博士基金资助项目(99547010D)。
【CateGory Index】: TQ426.94
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