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《Acta Chimica Sinica》 1988-08
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Preparation and Properties of the Molybdovanadophosphoric Acids with Dawson Structure

Wang En-Bo Gao Li-Hua Liu Jing-Fu Liu Zhong-Xu Yan De-Huan (Department of Chemistry,Northeast Normal University,Changchun)  
Five free molybdovanadophosphoric acids having Dawson sTructure were preparedby the use of an improved procedures The effect of reaction conditions on the formationof the five heteropolyacids has been studied.It was shown that the constitutions of theseheteropolyanions are[P_2Mo_(17)VO_(62)]~(7-),[P_2Mo_(16)V_2O_(62)]~(8-),[P_2Mo_(15)V_3O_(62)]~(9-),[P_2Mo_(14)V_4O_(62)H_2]~(8-),[P_2Mo_(13)V_5O_(62)H_2]~(9-).Thermogravjmetric and differentia]thermal analyses were performed on these hetero-polyacids.Potentiometric titration,IR,UV spectra and X-ray power diffraction werestudied.
【Fund】: 国家自然科学基金
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