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《Acta Chimica Sinica》 1994-01
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A Stopped-Flow Inductive Kinetic Spectrophotometric Method for Simultaneous Determination of Iron and Antimony

Wang, Jian-Hua He, Rong-Huan(Department of Chemistry, Yantai Teacher's College, Yantai, 264000)  
A stopped-flow inductive kinetic spectrophotometric method for the simultaneous determination of iron and antimony was proposed. The principle of determination was discussed, and a procedure for simultaneous determination of Fe(Ⅱ) and Sb (Ⅲ) was established based on the inductive effect of them on the chromium (VI)-iodide redox reaction. The calibration graphs were linear for 0-1.2μg·mL-1 Fe(Ⅱ)and 0-2.0μg· mL-1Sb(Ⅲ) respectively, and the detection limits were 0.012μg·mL-1 Fe(Ⅱ) and 0.014μg·mL-1 Sb (Ⅲ). The method was used for the determination of iron and antimony in zinc metal standard and a simulated sample, and the results are satisfactory.
【CateGory Index】: O657.3
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