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《Acta Chimica Sinica》 1999-10
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Highly Efficient Molecule Imprinting Chiral Stationary Phase Utilizing Combined Basic Functional Monomers

WANG Jin - Fang ZHOU Liang - Mo MENG Zi - Hui WANG Qing - Hai ZHU Dao - Qian ( Dalian Institute of Chemical Physics , The Chinese Academy of Sciences , Dalian, 116012 ) ( The People' s Liberation Army Academic of Military Medicine Sciences , Beijing, 100850 )  
Molecular imprinting polymers (MIP) against amino acid derivatives utilizing amide plus 2 -vinylpyridine as combined basic functional monomers were prepared and evaluated as chiral stationary phase for high - performance liquid chromatography. The MIPs prepared at optimized ratio of the imprinting molecule to combined functional monomers show excellent chiral separation ability to the imprinting enantiomer and its structurally related enantiomers. The effect of chemical group of the analyse on the chiral separation was investigated. Hydrogen bonding and strong ionic interaction between the functional monomer and the analyse were found.
【Fund】: 国家自然科学基金(29575212)资助项目
【CateGory Index】: O657.7
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