Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Acta Chimica Sinica》 2004-09
Add to Favorite Get Latest Update

Study of Paracetamol Molecularly Imprinted Polymers Applied to Solid Phase Extraction

HU, Shu Guo a WANG, Shan Wei b HE, Xi Wen , a ( a State Key Laboratory of Functional Polymer Materials for Adsorption and Separation Department of Chemistry, Nankai University, Tianjin 300071) ( b Center Lab of Nankai University, Tianjin 300071)  
Using paracetamol as an imprinted molecule, acrylamide as functional monomers, and EDMA as crosslinking agent, a polymer was prepared by molecular imprinting technique. The polymer was loaded into the self made solid phase extraction (SPE) cartridge. A SPE procedure was described for extracting and concentrating paracetamol using water and acetonitrile as the loading solvent. In order to optimize the washing and eluting solution, the adsorption of paracetamol in aqueous solution with the different percentage of methanol was studied. It was found that the paracetamol and two analogues (phenacetin and p tertiary butylphenol) were separated primely, and the paracetamol content in medicine (Endophy) was determined successfully, with the recovery being 94.3%.
【Fund】: 国家自然科学基金 (Nos.2 0 3750 1 7;2 0 1 750 0 9);; 天津市自然科学基金 (No.0 3360 351 1 );; 教育部博士点基金 (No.2 0 0 2 0 0 550 0 2 )资助项目
【CateGory Index】: O658
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
【References】
Chinese Journal Full-text Database 10 Hits
1 SHI Wei,FU Shao-ping and ZHU Jing-bo(School of Food Science and Technology,Dalian Polytechnic University,Dalian 116034);Molecularly imprinted silica nanospheres for solid-phase extraction of bisphenol A in canned food[J];Chinese Journal of Analysis Laboratory;2012-06
2 ZHANG Xiao-xu,YOU Hui-zhen,LI Wei,TONG Chang-qing,LI Wei,QU Min,JIN Qiao(Dalian Ocean University,Liaoning Danlian 116023,China);Synthesis and Application of Molecularly Imprinted Polymer[J];Guangzhou Chemical Industry;2012-09
3 WANG Jin,LEI Xiao,HE Wen-li,WANG Chao-li(College of Science,Hunan Agricultural University,Changsha 410128,China);Advances of Application of Molecular Imprinting Technology[J];Chemistry & Bioengineering;2006-04
4 ZHONG Sheng,YANG Li-cheng,LI Ai-min(State Key Laboratory of Pollution Control and Resource Reuse,Environmental Engineering Department of Nanjing University,Nanjing,Jiangsu 210093,China);The Research Development of Polar Organic Pollutants Extraction and Detection with Solid-phase Extraction Sorbents[J];The Administration and Technique of Environmental Monitoring;2008-01
5 Hu Shuguo Li Li He Xiwen **(State Key Laboratory of Functional Polymer Materials for Adsorption and Separat ion, Department of Chemistry, Nankai University, Tianjin 300071, China);Molecularly Imprinted Polymers: A New Kind of Sorbent with High Selectivity in Solid Phase Extraction[J];Progress In Chemistry;2005-03
6 MA, Xiang-Xia HE, Xi-Wen ZHANG, Mo LI,Wen-You ZHANG,Yu-Kui (Department of Chemistry, Nankai University, Tianjin 300071) (National Chromatographic Research and Analysis Center, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116011);Binding Selectivity and Permeation Characterization of Molecularly Imprinted Polymer Membranes with Paracetamol as Template[J];Acta Chimica Sinica;2006-23
7 FENG Yin-qiao1,2,ZHOU Ru-jin2,TANG Yu-bin1,HU Xin-xin1,2(1.College of Material Science and Engineering,Jiangsu University of Science and Technology,Zhenjiang 212003,China;2.Maoming College,Maoming 525000,China);Application of Molecular Imprinting Technique to Solid Phase Extraction[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2011-01
8 Fan,Cunhua Yang,Yiqun Zhao,Wei Xiao,Yu Luo,Jing Liu,Xiaoya*(The Key Laboratory of Food Colloids and Biotechnology,Ministry of Education,School of Chemical and Material Engineering,Jiangnan University,Wuxi 214122);Research on Amphiphilic Copolymer MIP Micelles Electrochemical Sensor[J];Acta Chimica Sinica;2013-06
9 LAN Li-xin(Hunan Chemical Industry Vocation Technology Institute,Zhuzhou,Hunan 412004,China);Study of molecularly imprinting technology and its application[J];Technological Development of Enterprise;2004-11
10 HAN Yan-ting,MA Jin-qin,YUE Xuan-feng,ZHANG Jing(Key Laboratory of Analytical Chemistry for Life Science of Shaanxi Province, College of Chemistry and Chemical Engineering, Shaanxi Normal University,Xi′an 710062,Shaanxi,China);Preparation of lysozyme based molecularly imprinted polymers and its chromatographic evaluation[J];Journal of Shaanxi Normal University(Natural Science Edition);2012-04
China Proceedings of conference Full-text Database 1 Hits
1 Zhu Qiujin,~aWang Liping~b,WU Shengfang~b,Joseph Wasswa~c Gu Xiaohong~b,Tang Jian~(b,c) a School of Life Sdence,Guizhou University,Cuiyang,550025,China b State Key Laboratory ofFood Science and Technology,Jiangnan University,Wuxi 214122,China c School of Food Science Jiangnan University,Wuxi 214122,China;Selectivity of molecularly imprinted solid phase extraction for sterol compounds[A];[C];2010
【Citations】
Chinese Journal Full-text Database 4 Hits
1 Zhou Jie, Han Hongyan, He Xiwen , Shi Huiming (Department of Chemistry, Nanism. University, Tianjin, 300071);Selective Enrichment and Direct Determination of Trace Drug by Solid-phase Extraction[J];Chinese Journal of Analytical Chemistry;1999-01
2 Wang Jinfang,Zhou Liangmo, Liu Xueliang,Wang Qinghai,Zhu Daoqian (Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116012);Tribasic Cross-linker Molecular Imprinted Chiral Stationary Phase[J];CHINESE JOURNAL OF ANALYTIEAL CHEMISTRY;2000-10
3 Liu Qin, Zhou Yongxin, Meng Zihui, Wang Qingqing, Hu Xuying, Liu Yintang (Beijing Institute of Pharmacology and Toxicology, Beijing 100850);Determination of Nerve Agent Degradation Products in Rice by Molecule Imprinting Polymer-Solid Phase Extraction and Capillary Electrophoresis[J];Chinese Journal of Analytieal Chemistry;2001-04
4 GUO Hong Sheng, HE Xi Wen , DENG Chang Hui, LI Yi Jun (Department of Chemstry, The Key Lab of Functional Polymer Materials for Adsorption and Separation, Nankai University, Tianjin 300071, China);Studies of Selective Enrichment and Recognized Characteristics of Paracetamol Molecular Template Polymer[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;2000-03
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 ZHU QiuJin~(1,2) GU XiaoHong~1 TANG Jian~(1) WANG LinXiang~1 FENG Yu~1 LI GaoYang~1(1.Key Laboratory of Food Science and Safety,Ministry of Education,Southern Yangtze University,Wuxi Jiangsu 214036;2.School of Life Science,Guizhou University,Guiyang Guizhou 550025;3.Testing & Analysis Centre,Southern Yangtze University,Wuxi Jiangsu 214036,China);Interaction of 17β-estradiol and its structural analogues with functional monomers[J];Journal of Beijing University of Chemical Technology(Natural Science Edition);2007-01
2 JIAO Feipeng HUANG Kelong YU Jingang PENG Xiahui ZHAO Xuehui NING Fengrong (College of Chemistry and Chemical Engineering,Central South University,Changsha 410083);Study on Process of Thermodynamics for Chiral Separation of Naproxen in Molecular Imprinting[J];Materials Review;2005-08
3 Zhou Jie (Department of Chemistry, Shandong Agricultural University, Tai'an 271018)Wang Shanwei; Guo Hongsheng; He Xiwen (Gentral Lab, Department of Chemistry Nankai University, Tianjin 300071);Enantiomeric Recognition of Continuous Molecularly Imprinted Polymer Rod Prepared by In-situ Method[J];CHINESE JOURNAL OF ANALYTIEAL CHEMISTRY;2000-03
4 Lai Jiaping, He Xiwen *, Guo Hongsheng (Department of Chemistry, Nankai University, Tianjin 300071) Liang Hong (Chemistry and Life College, Guangxi Normal University, Guilin 541004);A Review on Molecular Imprinting Technique[J];Chinese Journal of Analytieal Chemistry;2001-07
5 Hu Xiaogang~(1,2),Li Gongke~(*1)~1(School of Chemistry and Chemical Engineering,Sun Yat-sen University, Guangzhou 510275)~2(School of Chemistry and Environment,South China Normal University,Guangzhou 510631);Application of Molecular Imprinting Technique in Sample Pretreatment[J];Chinese Journal of Analytical Chemistry;2006-07
6 GUO Hong Sheng, JIA Yu Mei, CAO Xian Feng, HE Xi Wen(1. Department of Chemstry, Nankai University, Tianjin 300071, China);Synthesis of Molecularly Imprinted Microspheres Polymer with 4-Aminopyridine as Template and the Study of Their Binding Characteristics[J];Chemical Research In Chinese Universities;2001-03
7 YAN Liu\|Shui, WANG Yi\|Ming, WANG Zong\|Hua, LUO Guo\|An  (Department of Chemistry, Tsinghua University, Beijing 100084, China );Molecularly Imprinted Polymer Monoliths Prepared in Capillaries by Photoinitiated in situ Polymerization for the Screening of Caffeine[J];Chemical Research In Chinese Universities;2001-12
8 LI Qiu1,2,ZHANG Wei-ying1,LI Xiao1,LOU Jian-zhong1,3(1. College of Chemistry and Chemical Engineering,Fuzhou University,Fuzhou 350108,China; 2. Department of Chemical Engineering,Zhenjiang College,Zhenjiang 212003,China; 3. Department of Chemical Engineering,North Carolina Agricultural and Technical State University,Greensboro,NC 27411,U.S.A.);Synthesis and Properties of Salicylic Acid Surface Molecularly Imprinted Polymers from Aqueous Emulsions[J];Polymer Materials Science & Engineering;2010-08
9 CAO Bing-qing,PAN Yong,ZHAO Jian-jun,HUANG Qi-bin(Research Institute of Chemical Defence,Beijing 102205,China);Progress of the Applied Study on Imprinting Sensors and Preparation of Molecularly Imprinted Polymers[J];Chinese Polymer Bulletin;2007-08
10 LIU Peng,YUN Weixian,DONG Baolian,ZHOU Si,YANG Jiao,LING Yun,CAO Qiue(Key Laboratory of Medicinal Chemistry for Nature Resource,Ministry of Education,School of Chemical Science and Technology,Yunnan University,Kunming 650091,Yunnan,China);Study on the Influence of Functional Monomer on the Characteristics of Palladium(Ⅱ) Ion Imprinted Polymer[J];Precious Metals;2010-03
China Proceedings of conference Full-text Database 1 Hits
1 Zhou Shikun,Xu Danian (Research Institute of Chemical Defense,Beijing 102205);Analysis of 6 Degradation Products of Chemical Agents in Complex Organic Samples by GC/MS with n-SPE and Sylilation[A];[C];2011
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 Fan Jing,Liang Guozheng,Li Ling,Lan Liwen (Northwesten Polytechnical University,Xi'an 710072);ALLYL RESIN CONTAINING BORON MODIFIED BMI RESIN[J];Engineering Plastics Application;1997-01
2 Sheng Dekun~(1,2),Tan Juanjuan~(1,2),Liu Xiangdong~(1,2),Wang Pixin~1,Yang Yuming~1 (1.Key Laboratory of Polymer Ecomaterials,Changchun Institute of Applied Chemistry,Chinese Academy of Sciences,Changchun 130022,China; 2.Graduate School of the Chinese Academy of Sciences,Beijing 100049,China);MORPHOLOGICAL AND MECHANICAL PROPERTIES OF POLYURETHANE/MONTMORILLONITE NANOCOMPOSITES BY IN SITU POLYMERIZATION[J];Engineering Plastics Application;2011-11
3 XIA Ru 1,ZhANG Yu-chuan 1,YI You-min 2 YANG Ying-hai 2,YIN Shou-chun 1,WANG Ga 1,DONG Liang-wei 2 ( 1Department of Chemistry of Anhui University, Hefei 230039,China; 2Department of Physics of Anhui University, Hefei 230039,China);The Influence of Suspension Polymerization Conditions on the Diameter of Polymer Spherical Beads and Its Properties[J];Journal of Anhui University(Natural Sciences);2001-01
4 ZHOU Hui~1,LU Xiang-yang~1,TIAN Yun~1,HUANG Cheng-jiang~2(1 Laboratory of Biochemistry&Fermentation Engineering,HNAU,Changsha 410128;2 Yunnan Tobacco Academic Agricultural Institute,Yuxi 653100,China);Advances in Studies on Chemical Constituents and Pharmacological Activities of Apium L.[J];Amino Acids & Biotic Resources;2006-01
5 PAN Xiao-hui, LUO Wen-qian(The Chemistry & Life Science Department,Ankang Teachers College,Ankang 725000,China);The Studies on Chemical Constituents from the Root of Polgonum Cuspidatum in Ankang[J];Journal of Ankang Teachers College;2003-01
6 Li Lee Chen Boquan(Institute of Virology Chinese Academy of Preventive Medicine, Beijing );PRODUCTION OF BISPECIFIC MONOCLONAL ANTIBODIES ANTI-HFRSV-ANTI-HRP[J];Chinese Journal of Virology;1989-04
7 GAO Hong-qiu~1,SUN Jian~2(1.Agricultural Industrial And Commercial Scientific Research Institute Of Daqing Petrole Management Bureau,Daqing 163316,China;2.Daqing Environmental Monitoring Center Station,Daqing 163316,China);Gas Chromatography Mensurates Multifold Organic Phosphate Pesticide[J];North Environment;2005-06
8 Liang Yang,Song Zhiwei(College of Resource and Environment Engineering,Heilongjiang Institute of Science and Technology,Harbin 150027,China);Research and Development of Aerobic Granular Sludge in China and Abroad[J];Environmental Science and Management;2007-11
9 Ke Guang-ming 1 Wang Li 2 Du Hong-guang 1 Wang Shu-ming 2 Guo Hong-you 1 (1.College of Science, Beijing University of Chemical Technology, Beijing 100029; 2.Beijing KBD Pharmaceutical Technology Development Ltd,Beijing 100089, China);Measurement of lidocaine hydrochloride in patch by HPLC[J];Journal of Beijing University of Chemical Technology;2004-05
10 LUO Ai-qin,LIU Yun,WU Li-fei(School of Life Science,Beijing Institute of Technology,Beijing 100081,China);Synthesis and Selective Molecular Recognition of Hydrophilic Uridine Molecularly Imprinted Polymers[J];Transactions of Beijing Institute of Technology;2011-07
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 WANG Qiang,TAO Yu-gui,LI He-fei,LIU Hai-tao,CHEN Jing-ying(Dept.of Bioch.Engn.,Anhui University of Technology and Science,Wuhu 241000,China);Preparation,characterization of Pb~(2+)-imprinted hybrid membrane and investigation of its adsorption characteristic[J];Journal of Anhui University of Technology and Science(Natural Science);2008-04
2 LIAO Xiao-qiong,QIU Xiao-hui,YUAN Xiao-hong,LU Chuan-jian (The Second Clinical Medicine College of Guangzhou University of Chinese Medicine,Guangzhou 510120,China);Optimization the polymerization conditions of valsartan molecularly imprinted polymer[J];China Journal of Traditional Chinese Medicine and Pharmacy;2011-10
3 SONG Hong-xin,CHUAN Juan-juan,LIU Jing(Life Science & Engineering College,Shaanxi University of Science and Technology,Xi'an 710021,China);Resveratrol Extraction from Polygonum cuspidatum with Enzymic Dissolution[J];Acta Botanica Boreali-Occidentalia Sinica;2010-12
4 FU Ruo-nong(Department of Chemistry,Beijing Institute of Technoligy,Beijing 100081);Advances on SPE-chromatography in China in recent two years[J];Chinese Journal of Analysis Laboratory;2007-02
5 LIANG Xiao-yun,GUO Zhi-an*,WANG Dan-dan and ZHAO Jing-chan (Chemical Department of Northwest University,Xi′an 710069);Preparation of imidacloprid-imprinted polymer and its application as a solid phase extract[J];Chinese Journal of Analysis Laboratory;2008-05
6 LI Xiao-hong,CAO Yu-hua and GAO E-nuo(School of Chemical and Material Engineering,Jiangnan University,Wuxi 214122);Molecularly imprinted polymer microspheres for solid-phase extraction of methamidophos residue in milk[J];Chinese Journal of Analysis Laboratory;2009-06
7 Dan De-zhong,LENG Geng and HUANG Pu-xin(Department of Environmental Science and Engineering,Sichuan University,Chengdu 610065);Analysis of environmental samples[J];Chinese Journal of Analysis Laboratory;2010-07
8 ZHANG Zhaohui1,2,LIU Li1,NIE Lihua2(1 College of Chemistry and Chemical Engineering,Jishou University 416000)(2 State Key Laboratory of Chemo/Biosensing and Chemometrics,Hunan University,Changsha 410082);PREPARATION OF ERYTHROMYCIN-IMPRINTED SOLID-PHASE EXTRACTION MATERIAL BY SOL-GEL METHOD AND THE SELECTIVE ADSORPTION[J];Acta Polymerica Sinica;2010-06
9 HUANG Lei1,XIONG Zhouyi2,HE Pingsheng1,XIONG Hanguo1(1 College of Food Science and Technology,HuaZhong Agriculture University,Wuhan 430070)(2 Chutian College HuaZhong Agriculture University,Wuhan 430205);PREPARATION AND ADSORPTION CHARACTERISTICS OF MAGNETIC MOLECULARLY IMPRINTED POLYMER MICROSPHERES[J];Acta Polymerica Sinica;2011-01
10 PENG Yuan,FAN Yun-ge,MA Jian-biao (Key Laboratory of Functional Polymer Materials,Ministry of Education,Institute of Polymer Chemistry,Nankai University,Tianjin 300071,China);Polymer Sorbentsused for Solid Phase Extraction[J];Polymer Materials Science & Engineering;2007-04
China Proceedings of conference Full-text Database 2 Hits
1 Wang Zhonghua,Li Fuhua,Lin Changjiang,Zheng Yunsong (Beijing Institute of Microchemistry,Beijing 100091);Review on Liquid Explosives and the Detection Techniques[A];[C];2011
2 Chen Meixi,Yu Ziyou,Cao Xiaoqing,Sun Ting (Department of Chemistry,Northeastern University,Shenyang 110004);Synthesis and Adsorption Behavior of Sb(Ⅲ)-Imprinted Polymer Using Combination of Surface Imprinting Technique with Sol-Gel Method[A];[C];2011
【Secondary Citations】
Chinese Journal Full-text Database 8 Hits
1 Meng Zihui, Wang Qinghai, Zhu Daoqian, Zhou Liangmo (Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116012);Application of Molecular Imprinting in Chira1 Separation[J];Chinese Journal of Analytieal Chemistry;1997-03
2 Meng Zihui, Zhou Liangmo, Wang Jinfang, Wang Qinghai, Zhu Daoqian (Dalian Institute of Chemical Physics, Dalian ll60l2);Cmbined Interaction in Molecule Imprinting Chiral Stationary Phase[J];Chinese Journal of Analytieal Chemistry;1998-10
3 Liu Qin, Zhou Yongxin , Liu Yintang (Beijing Institute of Pharmacology and Toxicology, Beijing 100850);Recent Progresses in Research on Molecular Imprinting Sensors[J];Chinese Journal of Analytical Chemistry;1999-11
4 Liu Qin; Zhou Yongxin; Tang Lihe; Liu Yintang (Beijing,Institute of Pharmacology and Toxicology, Beijing 100850);Determination of Degradation Products of Six Nerve Agent by Capillary Zone Electrophoresis[J];Chinese Journal of Analytieal Chemistry;2000-07
5 ZHOU Jie, HE Xi Wen *, YANG Wan Long, SHI Hui Ming (Department of Chemistry, Nankai University, Tianjin, 300071);Studies on Character of Adsorption and Recognition of Etharidine Template Polymer[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;1998-09
6 ZHOU Jie, HE XiWen, ZHAO Jie, SHI HuiMing (Department of Chemistry, The Key Lab of Functional Polymer Materials for Adsorption and Separation, Nankai University, Tianjin, 300071);A Study of Binding Action and Selectivity of Trimethoprim Molecular Template Polymer[J];CHEMICAL RESEARCH IN CHINESE UNIVERSITIES;1999-02
7 WANG Jin - Fang ZHOU Liang - Mo MENG Zi - Hui WANG Qing - Hai ZHU Dao - Qian ( Dalian Institute of Chemical Physics , The Chinese Academy of Sciences , Dalian, 116012 ) ( The People' s Liberation Army Academic of Military Medicine Sciences , Beijing, 100850 );Highly Efficient Molecule Imprinting Chiral Stationary Phase Utilizing Combined Basic Functional Monomers[J];Acta Chimica Sinica;1999-10
8 MENG Zihui , WANG Jinfang , ZHOU Liangmo WANG Qinghai and ZHU Daoqian(Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian 116012, China);New cocktail functional monomers in making molecule imprinting polymer with high chiral selectivity[J];自然科学进展(英文版);1999-10
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved