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《Acta Chimica Sinica》 2004-09
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Study of Paracetamol Molecularly Imprinted Polymers Applied to Solid Phase Extraction

HU, Shu Guo a WANG, Shan Wei b HE, Xi Wen , a ( a State Key Laboratory of Functional Polymer Materials for Adsorption and Separation Department of Chemistry, Nankai University, Tianjin 300071) ( b Center Lab of Nankai University, Tianjin 300071)  
Using paracetamol as an imprinted molecule, acrylamide as functional monomers, and EDMA as crosslinking agent, a polymer was prepared by molecular imprinting technique. The polymer was loaded into the self made solid phase extraction (SPE) cartridge. A SPE procedure was described for extracting and concentrating paracetamol using water and acetonitrile as the loading solvent. In order to optimize the washing and eluting solution, the adsorption of paracetamol in aqueous solution with the different percentage of methanol was studied. It was found that the paracetamol and two analogues (phenacetin and p tertiary butylphenol) were separated primely, and the paracetamol content in medicine (Endophy) was determined successfully, with the recovery being 94.3%.
【Fund】: 国家自然科学基金 (Nos.2 0 3750 1 7;2 0 1 750 0 9);; 天津市自然科学基金 (No.0 3360 351 1 );; 教育部博士点基金 (No.2 0 0 2 0 0 550 0 2 )资助项目
【CateGory Index】: O658
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