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《Chemical Research and Application》 2007-12
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Hydrothermal synthesis and crystal structure of 1,4-dihydropyridine derivatives

WANG Jian-ping1,FU Yong-ju2,WANG Jian-ge1(1.Department of Chemistry,Luoyang Normal University,Luoyang 471022,China; 2.Chemical Engineering & Pharmaceutis College,Henan University of Science and Technology,Luoyang 471003,China)  
A series of 1,4-dihydropyridine derivatives were synthesized by the reaction of aromatic aldehydes,ethyl acetoacetate and ammonium bicarbonate under hydrothermal condition.Compared to the known report,this method has the advantages of excellent yields,convenience,less pollution and friendly environment.Compound b was deterimined by X-ray single-crystal diffraction.The crystal is of monoclinic,space group C2/c with a = 19.7348(12),b=7.4285(4),c = 27.2561(16),β=106.9950(10)°,V=0.38212(4)nm3,Z=8,Dc =1.236 Mg/m3,μ=0.085 mm-1,F(000)=1520,S=1.053,R=0.0574,wR=0.1732.
【Fund】: 洛阳师范学院重点学科资助课题
【CateGory Index】: O626.32
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【References】
Chinese Journal Full-text Database 1 Hits
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【Citations】
Chinese Journal Full-text Database 4 Hits
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【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 YIN Xiaogang;WU Xiaoyun;WANG Ye;CHEN Zhiming;CHEN Zhuo;Key Laboratory of Functional Materials Chemistry of Guizhou Province,School of Chemistry and Materials Science,Guizhou Normal University;;Ultrasonic assisted synthesis of 1,4-dihydropyridine derivatives in water[J];河北大学学报(自然科学版);2017-04
2 Pei Xuehai;Huang Kejun;Yin Xiaogang;Chen Zhiming;Key Laboratory of Functional Materials Chemistry of Guizhou Province,School of Chemistry and Materials Science,Guizhou Normal University;;Synthesis of 1,4-Dihydropyridine Derivatives Catalyzed by Pyrrolidine Organic Small Molecules[J];化学通报;2017-05
3 YIN Xiao-gang;WU Xiao-yun;WANG Ye;CHEN Zhi-ming;CHEN Zhuo;Key Laboratory of Functional Materials Chemistry of Guizhou Province,School of Chemistry and Materials Science,Guizhou Normal University;;Preparation of Hantzsch Ester Derivatives under Microwave Conditions[J];合成化学;2016-09
4 PEI Xue-hai;HUANG Ke-jun;CHEN Lin-yan;CHEN Zhi-ming;Key Laboratory of Functional Materials Chemistry of Guizhou Province,School of Chemistry and Materials Science,Guizhou Normal University;;Synthesis of Ion Compounds under Microwave Irradiation and Application in the Hantzsch Reaction[J];化学试剂;2016-04
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8 HE Yong1,CHEN Shiyun2,GAO Yonghao1,JIANG Hao1,WU Zonghao1(1.Hefei Huafang Pharmaceutical Science & Technology Co.,Ltd.,Hefei 230088; 2.Dept.of Chemical and Materials Engineering,Hefei University,Hefei 230022);Synthesis of Related Substances of Isradipine[J];中国医药工业杂志;2012-10
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【Co-references】
Chinese Journal Full-text Database 1 Hits
1 WANG Jian-ping1,FU Yong-ju2,WANG Jian-ge1(1.Department of Chemistry,Luoyang Normal University,Luoyang 471022,China; 2.Chemical Engineering & Pharmaceutis College,Henan University of Science and Technology,Luoyang 471003,China);Hydrothermal synthesis and crystal structure of 1,4-dihydropyridine derivatives[J];化学研究与应用;2007-12
【Secondary Citations】
Chinese Journal Full-text Database 2 Hits
1 SHI, Da-Qing ZHUANG, Qi-Ya CHEN, Jing WANG, Xiang-Shan, TU, Shu-Jiang HU, Hong-Wen (Department of Chemistry, Xuzhou Normal University, Xuzhou 221009) (Department of Chemistry, Nangjing University, Nangjing 210093);Reaction of Aromatic Aldehydes with 5,5-Dimethyl-1,3-cyclohexandione in Water[J];有机化学;2003-07
2 TU, Shu-Jianga ,a GAO, Yuan b YU, Chen-Xia a SHI, Da-Qing a ( aDepartment of Chemistry, Xuzhou Normal University, Xuzhou 221009) ( bDepartment of Chemistry, Shenzhen University, Shenzhen 518060);One Step Syntheseis of 4-Aryl-1,4-dihydroprydines by Using Microwave Irradiation Technology[J];有机化学;2002-04
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