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《West China Journal of Pharmaceutical Sciences》 2014-01
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Study on the purification procedure of Cassiae semen and Angelica dahuricae in Zhigui tablets

CHEN Xiao - liang;RUAN Jia;XU Chao - qun;YUAN Zhi - xiang;WANG Li - zhen;BIAN Jun - jie;College of Pharmacy,Chengdu University of Traditional Chinese Medicine;Sichuan Academy of Chinese Medicine Sciences;  
OBJECTIVE To study the purification process of Cassiae semen and Angelica dahuricae in Zhigui tablets. METHODS The extract rate of anthraquinone and imperatorin the yield rate of extract content were adopted. Compared with the ethanol,water precipitation,chitosan precipitation and adsorption method by macroporous resin. RESULT Compared with several purification methods,the acid- alkali method was selected for purification. The final purification process was as follows: adjust to pH6 with 20% lime milk,standing for 2 h,then filtered and dried under reduced pressure. CONCLUSION The acid- alkali method can meet formulation requirements for purification of anthraquinones component and imperatorin. The optimization process is simple and feasible,which provides technical basis for the study of the Zhigui tablets.
【Fund】: 四川省科研院所科技成果转化资金资助项目(No.11010120)
【CateGory Index】: TQ461
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