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《Pharmaceutical Journal of Chinese People's Liberation Army》 2008-02
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Preparation and Quality Standards of JM Saponin Sustained-Release Capsules

HUANG Yuan①②,CAI Guang-Ming②,ZHAO Huai-Qing,HOU Lu-Xing②③ (①College of Pharmacy ,Shenyang Pharmaceutical University, Shenyang 110016,Liaoning China) (②PLA Institute of Chinese Materia Medica,Hospital 302 of PLA,Beijing 100039 China) (③Department of Chemistry, Capital Normal University,Beijing 100037 China)  
Aim To prepare JM sustained-release capsules and establish a method for quality control.Methods The preparing technique of JM sustained-release capsules were optimized by the monofactorial design.The TLC was used in qualitative analysis and the HPLC was used for the quantitative analysis of JMGⅠand JMGⅡ.Results The spots in TLC were clear and distinguishable.The linear ranges of JMGⅠand JMGⅡ were 0.400~4.00μg(r=0.999 5) and 0.640~6.40μg(r=0.999 4),with average recovery rates at 103.4%(RSD=2.8%)and 102.1%(RSD=1.9%)(n=5), respectively.Conclusion The preparation of capsules was stable and the qualitative method was simple and quick.The qualitative result was accurate and reproducible.
【CateGory Index】: TQ461
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