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《Pharmaceutical Journal of Chinese People's Liberation Army》 2008-05
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Determination of Barbalion in XingnaoKukeya Tablet by HPLC

XIE Ling①,PAN Wei-Qin②,LI Xue-Qiang,LIU Xiao-Hui③,JING Jing④ (①Institute for Drug Control of Xinjiang Military Command,Wulumuqi 830063,Xinjiang China)(②Xinjiang Institute for Drug Control,Wulumuqi 830002,Xinjiang China)(③Integrated Warehouse Urumqi City,Wulumuqi 830002,Xinjiang China)  
Aim To develop a method for determination of barbalion in Xingnaokukeya tablets of Uygur medicine.Methods HPLC with Shimadzu ODS VP(4.6mm×250mm,5μm)column was used.The mobile phase consisted of acetonitrile-water(25∶ 75),with a flow rate of 1.0ml/min and detection wavelength at 360nm and under 30℃.Results The linear range was 0.238~2.38μg(r=0.999 9).The average recovery(n=9)was 98.80 % and RSD was 2.03%.Conclusion The method is simple,accurate,sensitive and could be used for quality control of the preparation.
【CateGory Index】: R29
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【Citations】
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1 MA Jing-jun~1,FANG Zheng~1,WU Qiu-hua~1,SUN Huan-ming~2,WEN Ya-jun~2(1.Agricultural University of Hebei,Baoding 071001, China;2.Beijing Agro-Tech Extension Station, Beijing 100029, China);On determination of Aloin and Aloe-emodin in Aloe barbadensis mill by HPLC[J];Journal of Agricultural University of Hebei;2005-02
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1 Liang Haiyan Sanjing Pharmaceutical Shareholding Co.,Ltd,Harbin Pharm.Group;Determination of the Content of Aloin of Baixuan Xiatare Tablets by HPLC[J];Heilongjiang Medicine Journal;2007-01
2 LU Chaoguo1),WANG Hongzhuan2),LI Yanhong1),LIU Guoji1),LUO Tingliang1) 1)Institute of Chemical Engineering,Zhengzhou University,Zhengzhou 450001 2)Nylon 66 Salt Company of China Shenma Group,Pingdingshan 467013;Simultaneous determination of Aloin and Aloe-emodin in Aloe by HPLC[J];Journal of Zhengzhou University(Medical Sciences);2008-03
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