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《Journal of Jilin University(Science Edition)》 2009-03
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Control of Solasedine Hydrochloride Quality

LI Li-ying1,FAN Jun-heng2,LIU Liang1(1.College of Chemistry and Biology,Beihua University,Jilin 132013,Jilin Province,China;2.Jilin University Press,Changchun 130021,China)  
High-perfomance liquid chromatography was used to study how to control solasedine hydrochloride quality.Column was Agilent ZORBAX Eclipse XDB-C18 column(150 mm×4.6 mm,5 μm),mobile phase was Vmethanol ∶Vacetonitrile ∶V0.020 mol·L-1lammonium acetate=60 ∶35 ∶5,flow rate was 1 mL/min,detection wavelength 205 nm,injection volume 10 μL,the solasodine hydrochloride quality separated from other impurities in a good linear range of 5~500 μg/mL(r=0.999 3),numder of theoretical plates n12 000(R1.5);the average recovery for the sample 98.6%(n=9).Relative standard deviation of reproducibility(RSD) was 0.618%.
【Fund】: 国家自然科学基金(批准号:20472016)
【CateGory Index】: R927
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