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《Journal of Jilin University(Science Edition)》 2009-03
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Control of Solasedine Hydrochloride Quality

LI Li-ying1,FAN Jun-heng2,LIU Liang1(1.College of Chemistry and Biology,Beihua University,Jilin 132013,Jilin Province,China;2.Jilin University Press,Changchun 130021,China)  
High-perfomance liquid chromatography was used to study how to control solasedine hydrochloride quality.Column was Agilent ZORBAX Eclipse XDB-C18 column(150 mm×4.6 mm,5 μm),mobile phase was Vmethanol ∶Vacetonitrile ∶V0.020 mol·L-1lammonium acetate=60 ∶35 ∶5,flow rate was 1 mL/min,detection wavelength 205 nm,injection volume 10 μL,the solasodine hydrochloride quality separated from other impurities in a good linear range of 5~500 μg/mL(r=0.999 3),numder of theoretical plates n12 000(R1.5);the average recovery for the sample 98.6%(n=9).Relative standard deviation of reproducibility(RSD) was 0.618%.
【Fund】: 国家自然科学基金(批准号:20472016)
【CateGory Index】: R927
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【References】
Chinese Journal Full-text Database 2 Hits
1 LI Fu-ren1,CHOU Li-li2,LIU Liang3(1.Basic Medical College of Beihua University,Jilin 132013,China; 2.Medical Inspection College of Beihua University,Jilin 132013,China; 3.Chemistry and Biology College of Beihua University,Jilin 132013,China);Effect of Solasodine Hydrochloride Injection on Lewis Lung Tumor of Mice[J];Journal of Beihua University(Natural Science);2011-01
2 LI Fu-ren1,CHOU Li-li2,LIU Liang3(1.Basic Medical College of Beihua University,Jilin 132013,China;2.Medical Inspection College of Beihua University,Jilin 132013,China;3.Pharmacy College of Beihua University,Jilin 132013,China);Inhibitory Effects of Solasodine Hydrochloride on Liver Cancer H_(22) in Mice[J];Journal of Beihua University(Natural Science);2011-03
【Citations】
Chinese Journal Full-text Database 10 Hits
1 TANG,Xiao-Meia XU,Qi-Haib WANG,Jinga LIN,Jing-Rong,a JIN,Rong-Huaa TIAN,Wei-Sheng,a,b(a The Laboratory of Resource Chemistry,Shanghai Normal University,Shanghai 200234)(b Shanghai Institute of Organic Chemistry,Chinese Academy of Sciences,Shanghai 200032);Synthesis of Solasodine by Using the Intact Skeleton of Diosgenin[J];Acta Chimica Sinica;2007-20
2 LU Jia-hui, JIANG Chao-jun, MENG Qing-fan, GAO Chao-hui, WEI Wei, ZHAO Hang, TENG Li-rong(Department of Biopharmacy, College of Life Science, Jilin University, Changchun 130012, China);Determination of Methanol and Ethanol in Ternary Mixture by Near Infrared Spectroscopy with PLS Regression[J];Journal of Jilin University (Science Edition);2005-03
3 LI Wen-liang~1,MI Hong~2,DOU Ying~1,CHEN Yong-hong~1,WANG You-bing~3,REN Yu-lin~1 (1.College of Chemistry,Jilin University,Changchun 130021,China;2.Pharmaceutical Research Center,Jilin Institute of Traditional Chinese Medicine,Changchun 130021,China;3.Department of Chemistry,Baicheng Medical College,Baicheng 137000,Jilin Province,China);Application of Near-infrared Diffuse Reflectance Spectroscopy in Controlling Extractant of Cnidium Monieri by Supercritical CO_2[J];Journal of Jilin University(Science Edition);2006-04
4 YANG Hui~1,CHEN Xiao-qing~(1),ZHAO Yu~2,XUE Xiao-juan~1 (1.Department of Chemistry and Chemical Engineering,Central South University,Changsha 410083,Hunan,China;2.ChangHong Medicine Research Company,Zhuhai 519085,Guangdong,China);Analysis of Steroidal Alkaloid and Research of Its Formation and Transformation in Solalum Nigrum L.[J];Fine Chemicals;2006-04
5 CHEN Yuan-yuan,WU Xiao-jing,LI Fa(School of Chemical Engineering,Hefei University of Industry,Hefei 230009,China);Infrared Spectrometric Study on Solvation Property of Methanolic Solution of Calcium Chloride[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2008-04
6 JIANG Xin-yu1,YANG Hui1,*,ZHAO Yu2(1.College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,China;2.Changhong Medicine Research Company,Zhuhai 519085,China);The Determinnation of Steroidal Alkaloid Content in Solanum nigrum L[J];Food Science;2006-08
7 WU Xiao Feng1 SHI He Ping1 TSANG Po Keung Eric2(1College of Life Sciences,South China Normal University,Guangdong Provincial Key Lab of Biotechnology for Plant Development,Guangzhou 510631,P.R.China;2Department of Mathematics,Science,Social Science and Technology,The Hong Kong Institute of Education,Hong Kong,China);INDUCTION AND IN VITRO CULTURE OF HAIRY ROOTS OF SOLANUM NIGRUM L. VAR. PAUCIFLORUM LIOU AND ITS SOLASODINE PRODUCTION[J];Journal of Molecular Cell Biology;2008-03
8 GU Jin-hua,ZHANG Wei,LI Feng,WANG Yu-qin,XU Ji-liang~*,SHAO Zheng-yi(Basic Medical College,Nantong University,Nantong 226001,China);The Antineoplastic Effect of Solanum nigrum Compound Capsule and Its Influence on Tumor Cell Cycle[J];LiShiZhen Medicine and Materia Medica Research;2006-12
9 LIU Qin,CHEN Xiao-qing*,JIANG Xin-yu,WU Sheng-de(College of Chemistry and Chemical Engineering,Central South University,Changsha 410083,China);Study on the Microwave-Assisted Extraction of the Total Steroidal Alkaloids from Solanum nigrum L.[J];Natural Product Research and Development;2005-01
10 LI Ming-Hui1,2,DING Gang2,MENG Zhao-Qing2,CAI Jing2,LIU Jing-Jing11School of Life Science & Technology, China Pharmaceutical University,Nanjing 210009;2Jiangsu Provincial Center for Chinese Medicine Quality Control,Nanjing 211100,China;Content Determination of Solasonine and Solamargine in Solanum nigrum[J];Chinese Journal of Natural Medicines;2007-05
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 WU You-ji,JIN Ying,HU Zhang-wen,ZHOU Wei(Dept.of Bioch.Engn.,Anhui University of Technology and Science,Wuhu 241000,China);The Preparation of Nano-ZnS/AOCF[J];Anhui Chemical Industry;2006-05
2 LIU Chun-hua et al(Analysis and Test Center of Chinese Academy of Tropic Agriculture Sciences,Haikou,Hainan 571101);Research Progress of Solanine in the Potato and Its Products[J];Journal of Anhui Agricultural Sciences;2010-07
3 BO Li-li et al (Gansu Key Lab of Crop Improvement and Germplasm Innovation,Gansu Agricultural University,Gansu Key Laboratory of Aridland Crop Science,Lanzhou,Gansu 730070);Study on Extraction of Glycoalkaloids in Potato[J];Journal of Anhui Agricultural Sciences;2012-03
4 ZHANG Jun-xiang,GAO Song-ping,WANG Zhi-yu(Department of Applied Chemistry,Taiyuan Institute of Technology,Taiyuan 030008,Shanxi,China);Research on the Synthetic Technology of 1,1′Diacetylferrocene[J];Acta Armamentarii;2008-04
5 LI Xiao-ying,DENG Wen-yi,WU Ying-ying,HE Wei(School of Photoelectric Information and Telecommunication Engineering, Beijing Information Science and Technology University,Beijing 100101,China);Identification of plastic based on infrared spectrum[J];Journal of Beijing Information Science & Technology University;2011-03
6 Liu Shuzhi,Xu Shurong Editorial Board of Journal of Chinese Mass Spectrometry Society,102413,Beijing,China;Some mass quantities and their units in mass spectrometry[J];Acta Editologica;2005-05
7 XIE Jian-chun,SUN Bao-guo,SHA Shuang,ZHENG Fu-ping,DANG Wan-bin(College of Chemical and Environmental Engineering,Beijing Technology and Business University,Beijing 100037,China);STUDY ON SYNTHESIS OF FOOD FLAVOR 4-PENTENOIC ACID[J];Journal of Beijing Technology and Business University(Natural Science Edition);2007-01
8 Li Liying(College of Chemistry and Biology Science,Beihua University,Jilin 132013,P.R.China);Sun Liguang(Qingdao Tumor Hospital);Liu Liang(Beihua University);Content Determination for Solasodine Hydrochloride in Preparation of Morel[J];Journal of Northeast Forestry University;2009-06
9 XU Liang-zheng,LI Kun-xin,LIAO Fu-lin,LIU Hui-na,YANG He-sheng(School of Life Science,Jiaying University,Meizhou,Guangdong 514015,China);Seeds Germination and Juice Allelopathy of Solanum nigrum L. var. pauciflorum Liou[J];Acta Botanica Boreali-Occidentalia Sinica;2009-10
10 YI Gui-Yuan,CAO Chen-Zhong(School of Chemistry and Chemical Engineering,Hunan University of Science and Technology,Xiangtan 411201);Influence of Electronegativity,Polarizability and Steric Effects on the ~(13)C Nuclear Magnetic Resonance Chemical Shift of Aliphatic Amines[J];Chinese Journal of Analytical Chemistry;2009-02
China Proceedings of conference Full-text Database 1 Hits
1 Liu Aimin~1 Wang Min~1 Huang Weiyi~2 1 College of Life Sciences,Anhui Normal University,Wuhu,241000,China 2 College of Life Sciences,Nanjing Agriculture University,Nanjing,210095,China;Effects of antibiotics on the cadmium-tolerant capability of a Pseudomonas strain and IR spectroscopy analysis[A];[C];2008
【Co-references】
Chinese Journal Full-text Database 10 Hits
1 LIU Liang 1,2 ,ZHOU Shou-biao 1,ˇ ,ZHENG Wei-fa 2 (1.Provincial Key Laboratory of Conservation and Exploitation of Biological Resources in Anhui,Institute of Life Science,Anhui NormalUniversity,Wuhu Anhui241000,China;2.Provincial Key Laboratory of Biotechnology on Medical Plants,Xuzhou Jiangsu221116,China);Inhibition of Tumor Cells by Ethanol Extract of Fomes Fomentarius[J];Carcinogenesis,Teratogenesis and Mutagenesis;2005-02
2 XU Du-juan,CHEN Min-zhu (The Department of Pharmacy,the First Affiliated Hospital of Anhui Medical University,Anhui Hefei 230022, China);Protection of Total Astragalus Extract Against Chemotherapy-induced Leukopenia and Immunosuppression in Tumor Bearing Mice[J];Journal of Anhui Traditional Chinese Medical College;2006-03
3 JIANG Chao, QING Chen, MENG Ling hua, et al. Shanghai Institute of Material Medical,Chinese Academy of Sciences,Shanghai 200031,P.R.China;Inhibitory effects of China ganoderma lucid essence (CGLE) on DNA topoisomerases and its ability to induce apoptosis of K562 cells[J];CHINESE JOURNAL OF CANCER;1999-06
4 FU Zhao Di, CAO Yu, WANG Kai Feng, XU Shao Feng, HAN Rui Institute of Materia Medica, Chinese Academy of Medical Sciences and Peking Union Medical College, Beijing 100050, P.R.China;Chemopreventive Effect of Resveratrol to Cancer[J];Chinese Journal of Cancer;2004-08
5 AI Jin-Xia, LIU Liang, WANG Bing-Mei Department of Immunology, Medical College of Beihua University, Jilin 132013, China;Influence of growth inhibition on HeLa cells by SBHL[J];Journal of The Fourth Military Medical University;2004-19
6 LI Fu-ren,LIU Liang.(Beihua University,Jilin 132013,China);EXPERIMENTAL STUDY OF SOLASODINE HYDROCHLORIDE ON THE GROWTH OF HELA CELLS IN VITRO[J];Modern Preventive Medicine;2008-19
7 AI Jin-xia(Inspect College of Beihua University,Jilin 132013,China);Experimental Investigation Derived from Sdosodine Hydrochlorida on Apoptosis of the Cervical Cancer Cells[J];Journal of Beihua University(Natural Science);2008-01
8 LI Li-ying (Chemistry and Biology College of Beihua University,Jilin 132033,China);Determination of Solasodine Hydrochloride by Using Ultraviolet-Visible Spectrophotometry[J];Journal of Beihua University(Natural Science);2009-01
9 LI Li-ying1,SUN Li-guang2,FAN Jun-heng3,LIU Liang1(1.Chemistry and Biology College of Beihua University,Jilin 132033,China;2.Tumor Hospital of Qinhuangdao City,Qinhuangdao 066000,China;3.Publishing House of Jilin University,Changchun 130012,China);Analysis of IR Characterization for Solasodine Hydrochloride[J];Journal of Beihua University(Natural Science);2009-02
10 LIU Yan-bo1,GENG Yan2,GE He1,LU Li-li1 (1.Basic Medical College of Beihua University,Jilin 132013,China;2.Disease Prevention and Control Center of Fengman District in Jilin City,Jilin 132013,China);Construction of Survivin siRNA Expression Vector and the Inhibition Effects on Prostate Neoplasm DU145 Cell Growth[J];Journal of Beihua University(Natural Science);2010-02
【Secondary References】
Chinese Journal Full-text Database 1 Hits
1 LIU Xiao-Bo;ZHANG Yang;WANG Li;College of Life Sciences,Sichuan University;;GC-MS analysis of total alkaloids in Liparis nervosa(Thunb.)Lindl.[J];Journal of Sichuan University(Natural Science Edition);2015-04
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 ZHANG Jun1,ZHENG Yongmei2,WANG Fangrong3,CHEN Xingdan1e of Optics, Fine Mechanics and Physics,Chinese Academy of Sciences, Changchun 130022,China;2College of Physics,Jilin University, Changchun 130025,China;3College of Communication and Engineering, Jilin University, Changchun 130012,China) ;Discussion on some regular methods for cereal near infrared spectra analysis[J];Journal of Changchun Post and Telecommunication Institute;2003-01
2 AI Jin-Xia, LIU Liang, WANG Bing-Mei Department of Immunology, Medical College of Beihua University, Jilin 132013, China;Influence of growth inhibition on HeLa cells by SBHL[J];Journal of The Fourth Military Medical University;2004-19
3 Yang Nanlin, Cheng Yiyu *, Qu Haibin (Department of Chinese Medicine Science & Engineering, Zhejiang University, Hangzhou 310027);Quantitative Determination of Mannitol in Cordyceps Sinensis Using Near Infrared Spectroscopy and Artificial Neural Networks[J];Chinese Journal of Analytical Chemistry;2003-06
4 Wu Xiaohua *, Chen Dezhao (Department of Chemical Engineering, Zhejiang University, Hangzhou 310027);Recent Development of Non-linear Patrital Least Squares in Chemometrics[J];Chinese Journal of Analytical Chemistry;2004-04
5 JI Yu-Bin, WANG Sheng-hui, GAO Shi-yong, JI Chen-feng, ZOU Xiang, WANG Shuai-shuai (Postdoctal Research of Institute of Materia Medica,Harbin University of Commerce,Harbin 150076, China);Study on active composition of solanum nigrum L.(SNL)[J];Journal of Harbin University of Commerce(Sciences Edition);2004-06
6 Ren Yulin; Li Wei; Guo Ye (Department of Chemistry, Jilin University, Changchun, 130023)Ren Yuqiu (Baicheng Health School, Baicheng, 137000)Zhang Lu; Sun Ying; Chen Bo (Department of Pharmacy, Changchun Medical College, Changchun, 130031);Noninvasive Analysis of Analgini by PLS-Near-infrared Diffuse Reflectance Spectroscopy[J];ACTA SCIENTIARIUM NATURALIUM UNIVERSITATIS JILINENSIS;1997-03
7 HE Shu hua, SUN Rui yan, REN Yu qiu, WANG Hong feng, WANG Wen long, WANG Li li (Changchun College of Traditional Chinese Medicine, Changchun, 130021, P.R.China);Classifying Ginseng According to Near Infrared Diffuse Reflection Spectrum[J];Acta Scientiarium Naturalium Universitatis Jilinensis;2001-01
8 GUO Ye, GOU Yu-hui, REN Yu-lin (Department of Chemistry, Jilin University, Changchun, 130023, P.R.China) TANG Zen, LIU Fu-qiang, TIAN Li-rong (Pharmacy, 208th Hospital of PLA, Changchun, 130061, P.R.China);Nondestructive Quantitative Analysis of Sulfamethoxazole[J];Acta Scientiarium Naturalium Universitatis Jilinensis;2001-02
9 LU Jiahui, TENG Lirong, JIANG Fuming, REN Yulin(College of Chemistry, Jilin University, Changchun 130023, China)QIU Fangping(Colloge of Bioengineering, Changchun Industrial University, Changchun 130012, China)WANG Youbing(Bacheng Medical College, Baicheng 137000, China);Rapid Determination of Ethanol in Wine by Short-wavelength Near-infrared Spectroscopy[J];Acta Scientiarium Naturalium Universitatis Jilinensis;2003-02
10 LU Jia-hui, JIANG Chao-jun, MENG Qing-fan, GAO Chao-hui, WEI Wei, ZHAO Hang, TENG Li-rong(Department of Biopharmacy, College of Life Science, Jilin University, Changchun 130012, China);Determination of Methanol and Ethanol in Ternary Mixture by Near Infrared Spectroscopy with PLS Regression[J];Journal of Jilin University (Science Edition);2005-03
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