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《Journal of Jishou University(Natural Sciences Edition)》 2010-02
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Determination of Trace Vanadium in Vanadium-ExtractionWaste Water by Catalytic Kinetic Photonmetry-V(Ⅴ)-KIO_4-Methyl Red System

SHI Mei-lian,DUAN You-gou,YAN Wen-bin,REN Cong-lian(College of Chemistry and Chemical Engineering,Jishou University,Jishou 416000,Hunan China)  
Based on the catalytic effects of Vanadium(Ⅴ) on the discoloring reaction of methyl red oxidized by KIO4 and methyl red in a medium of citric acid,a new method for the determina-tion of vanadium by catalytic kinetic spectro-photometry was proposed.Linear relationship between log(A0/A) and the concentration of vanadium is observed in the range of 0.64~3.2 μg/mL.The limit of detection is 3.75×10-3μg/mL.The proposed method has been used satisfactorily in the determination of vanadium in vanadium-extraction waste water.
【Fund】: 湖南省科技计划项目(2006GK4012)
【CateGory Index】: O657.3;X832
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