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《Journal of Jiangsu Polytechnic University》 2008-03
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Conductivity of Polyaniline/Attapulgite Nanocomposites Doped by H_3PO_4

WU Feng-qin1,ZENG Yong-bin1,YAO Chao1,LI Xiao-tang2,XU Qi-li3(1.Analysis Center,Jiangsu Polytechnic University,Changzhou 213164,China;2.Jiangsu Engineering Technology Research Center of Attapulgite,Xuyi 211700;3.Changzhou Huazhu Pigment Co.,Ltd.,Changzhou 213016)  
The surface of attapulgite was encapsulated with the PANI doped with phosphate acid(H3PO4) to synthesize the H3PO4-PANI/ATP nanocomposites by in situ polymerization method.The effect of the polymerization time,the amount of H3PO4,the amount of Ammonium persulfate(APS),the polymerization temperature and the dosage of aniline on the volume resistivity were studied.The result indicated: when the polymerization temperature was 20 ℃,the dosage of aniline was 30%,the polymerization time was 4 h,the molar ratio of An,APS and H3PO4 was 1∶1∶5.81,the volume resistivity of nanocomposites could reach 6 Ω·cm.The nanocomposites prepared on this condition was also characterized by XRD,FTIR and TG-DTA.
【Fund】: 江苏省富民强县(BE2006373);; 常州市科技攻关(CE2007075 CE2008077)
【CateGory Index】: TB383.1
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