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《Acta Metallrugica Sinica》 1994-14
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PREPARATION OF Ni-Al INTERMETALLIC COMPOUNDS BY MECHANICAL ALLOYING

LI Gusong;DING Bingzhe;MIAO Weifang;YE Lilei;GUO Jianting(State Key La boratory of RSA,Institute of Metal Research,The Chinese Academy of Sciences,Shenyang)(Manuscript received 30 June,1993;in revised form 18 August,1993)  
The powder mixtures of Ni and Al with compositions of Ni50 at.-% Al and Ni-25 at.-% Al as well as Ni_3Al alloy powder were milled in a Spex 8000 Mixer/Mill respectively.After 3 h of milling,Ni-50 at.-%Al mixture transforms into NiAl with grain size of about 5 nm,while after 5 h,Ni-25 at.-%Al mixture transforms into disordered metastable Ni solid solution.As to the Ni_3Al alloy powder,5 h milling makes its structure change from Ll_2-type intermetallic compound with long range order into fcc disordered solid solution;further milling results in the formation of nanocrystalline structure.
【Fund】: 国家自然科学基金 国家科委八六三项目
【CateGory Index】: TF124
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