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《Bulletin of the Academy of Military Medical Sciences》 2010-03
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Chemical constituents of Galium aparine

LI Jian,LI Bing,CHEN Li,LIU Shi-jun,DONG Jun-xing(Institute of Radiation Medicine,Academy of Military Medical Sciences,Beijing 100850,China)  
Objective To investigate the chemical constituents of 60% alcohol extract of Galium aparine L.Methods The compounds were isolated by column chromatography over silica gel and Sephadex LH-20 coupled with preparative silica gel TLC.Structures of the compounds were elucidated on the basis of physicochemical properties and spectral data.Results Eleven compounds were isolated and identified as 4-hydroxybenzoic acid(1),vanillic acid(2),protocatechuic acid(3),cytosine(4),cytidine(5),uracil(6),uridine(7),adenosine(8),xanthopurpurin(9),2-methyl-1,3,6-trihydroxy-9,10-anthraquinone-3-O-α-rhamnosyl(1→2)-β-D-glucoside(10),2-carbomethoxy-3-prenyl-1,4-naphthohydroquinone-di-O-β-D-glucoside(11),respectively.Conclusion Compounds 1-11 are isolated from this plant for the first time.
【CateGory Index】: R284
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