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《Fine Chemicals》 2006-06
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Preparation and Characterization of Polyaniline/Nano-ATO Conductive Composite Materials

ZHAO Ge,FU Xiang-kai,MA Li-hua(The Key Laboratory of Applied Chemistry of Chongqing Municipality,Research Institute of Applied Chemistry,College of Chemistry and Chemical Engineering,Southwest China University,Chongqing 400715,China)  
A composite of polyaniline(PANI) containing antimony doped tin oxide nanoparticles(nano-ATO) was prepared by in situ polymerization method.Dodecyl-benzenesulfonic acid(DBSA) and hydrochloric acid were used as dopant and ammonium persulfate(APS) was used as oxidant during the polymerization.The effect of content of nano-ATO on the conductivity of the composite material was studied.When n(aniline)∶n(APS)∶n(DBSA)=1∶1∶0.7 and m(ATO)∶m(aniline)=0.1∶1,the highest conductivity was 8.35 S/cm at 25 ℃,which raised one order of magnitude compared with that of PANI synthesized by the conventional method and two orders of magnitude compared with that of nano-ATO.The PANI/nano-ATO composite materials were characterized by FTIR,XRD,SEM and TEM.The results indicated that aniline polymerizes preferentially on the surfaces of nano-ATO,resulting in polyaniline coated nano-ATO conductive composite materials(PANI/nano-ATO).
【CateGory Index】: TB332
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