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《Advances in Fine Fetrochemicals》 2002-09
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Study of Steam Stripping Process during Synthesis of 3 - Chloro - 2 - Hydroxypropyl Trimethyl Ammonium Chloride

Wang Fenghe Wang Jing Lei Wu Xia Mingzhu Wang Fengyun (Industrial Chemistry Institute , NUST, Nanjing 210094)  
The refining process to synthesize 3 - chloro - 2 - hydroxypropyl trimethyl ammonium chloride ( CHPT-MA) from trimethyl amine, HC1 and epichlorohydrin as raw materials was studied. Effects of ratio of steam to reactants , feeding temperature, vacuum pressure and vapor pressure on the reaction were examined. The optimum reaction conditions were detennined as follows: vacuum pressure 0.070 - 0.075 MPa, ratio of steam to reactants 1.55 -1.65, vapor pressure 0.3 MPa with feeding under room temperature. The content of CHPTMA was 48 % - 52 % , DCH as impurity in reaction system was no more than 20 ppm.
【CateGory Index】: TQ226
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