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《ACTA MINERALOGICA SINICA》 1997-02
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SYNTHESIS AND CHARACTERIZATION OF PILLARED MONTMORILLONITE

Wu Pingxiao; Zhang Huifen; Xiao Wending; Wu JingPing (Guangzhou Institute of Geochemistry, Chinese Asademy of Sciences, Guangzhou, 51O64O) (Department of Applied Chemistry, China University of Geosciences, Wuhan, 43O074)  
This paper employs several methods to synthesize Keggin ioas,and finds the fitting acidi-ty and alkalinity-mild or medium alkalinity to synthesize stable Keggin ions. These pillared agentsare used to synthesize the pillared montmorillonite with basal interlayer spacing 2. 4～2. 5nm. Thepillared montmorillonite was identified by XRD, IR, and DTA in this paper. The surface physico-chemical properties were determined by BET and Py-IR. The results have shown that it is suitableto use Keggin ions to synthesize the pillared montmorillonite with basal interlayer spacing 2. 4～2. 5nm, and after incandescing at 35OC, the basal interlayer spacing is stabilized 1. 8nm, with alarger space surface area and a Lewis acidity centre.
【Fund】： 广东省自然科学基金
【CateGory Index】： P578
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