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《Journal of Mineralogy and Petrology》 2009-02
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LIU Xiao-wen,LIU Zhuang,ZHONG Gang,MAO Xiao-xi School of the Resources Processing and Bio-engineering,Central South University,Changsha 410083,China  
Zr/Al-pillared montmorillonite was prepared by using Na-montmorillonites as starting materials.The effect of Zr/Al molar ratio and measurement of NaOH on Zr/Al pillared montmorillonite was investigated.Characterization by XRD indicated that when the molar ratio of Zr4+ and Al3+ was 1∶6 and the volume of 0.4 mol/L NaOH was 70 ml,the d(001)value of the pillared montmorillonite reached maximum.The FT-IR results of Zr/Al-montmorillonite showed that the Zr/Al polyoxocations had already inserted into the interlayer of montmorillonite and formed the band of Si—O—Al and Si—O—Zr.BET analysis showed Zr/Al-montmorillonite had larger specific area and smaller pore distribution.This study indicated that it was a useful catalysis and absorbent adsorbent materials
【Fund】: 973国家重大基础研究项目(2005CB623701)
【CateGory Index】: TD985
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