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《Bulletin of Mineralogy, Petrology and Geochemistry》 2007-02
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Experimental Study on Preparation of Grossular Glass-ceramics from Red Mud

XING-Jing, LI Jin-Hong, Zhang-KaiNational Laboratory of Mineral Materials, China University of Geosciences, Beijing 100083, China  
The glass-ceramics have been prepared through sintering of red mud and quartz sand. The based glasses were obtained by melting materials of designed batch at 1300℃, and then were milled, sieved, and then were used to prepare grossular glass-ceramics through double heating treatment. XRD and SEM were applied to study the red mud and glass-ceramics. The results showed that the red mud is mainly composed of calcite and aragonite. The properties of glass-ceramics and the crystal structure of grossular are relative strongly affected by the heating temperature. The optimum condition for the preparation of grossular glass-ceramics is nucleating at 900℃ for 1 hour and crystallizing at 1105℃ for 2 hours. The glass-ceramics prepared under this condition contain high crystal contents with euhedral crystals, good properties, bulk density of 2.79 g/cm3 , and micro hardness of 6.52.
【Fund】: 国家自然科学基金资助项目(40602008);; 矿物材料国家专业实验室开放基金资助项目(A05005)
【CateGory Index】: P579
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