Full-Text Search:
Home|Journal Papers|About CNKI|User Service|FAQ|Contact Us|中文
《Physical Testing and Chemical Analysis Part B Chemical Analysis》 2005-12
Add to Favorite Get Latest Update


WANG Lian-zhu~1,YOU Jun~1,CHEN Zhi-hua~1,LIANG Ming~2,LU Shen-yu~2,HONG Wei-ping~1(1.Zhangzhou Entry-Exit Inspection and Quarantine Bureau,Zhangzhou 363000,China;2.Fujian Entry-Exit Inspection and Quarantine Bureau,Fuzhou 350001,China)  
Gas chromatography hyphenated with solid-phase extraction was applied to the rapid determination of 8 residual organophosphorus pesticides(Opp′s) in welsh onion.The onion sample(25 g) was extracted with a mixture containing 50 mL of acetonitrile and 10 mL of sat′d NaCl water solution.The extract was filtered and salted out with 6 g of NaCl by shaking vigorously for 3 min in a separatory funnel.10.0 mL of the organic phase was evaporated(at 40 ℃) to dryness,and the residue was taken up with 1.0 mL of nhexane,and purified by SPE on silica gel column(Accu Bond Ⅱ silica cartridges).The Opp′s on the column was eluted with acetone-n-hexane((1+1)) mixture and 15 mL of the eluate was taken and dried by blowing with nitrogen.n-Hexane(1.0 mL) was used to dissolved the residue and the solution was used for GC determination.Two capillary columns(HP 5 and DB1701) with different polarity were used in the GC identification and determination,and two flame photometric detectors were used.Recoveries for the 8 Opp′s were tested by the standard addition method and the results obtained were in the range of 60%-130%.RSD′s found were less than 18%.Detection limits were in the range of 0.02-0.05 mg·kg~(-1).
【CateGory Index】: TS207.53;O657.71
Download(CAJ format) Download(PDF format)
CAJViewer7.0 supports all the CNKI file formats; AdobeReader only supports the PDF format.
Chinese Journal Full-text Database 7 Hits
1 FU Ruo-nong(Department of Chemistry,Beijing Institute of Technoligy,Beijing 100081);Advances on SPE-chromatography in China in recent two years[J];Chinese Journal of Analysis Laboratory;2007-02
2 WANG Lian-zhu,HU Chao-yang,ZHENG Jun-chao,YOU Jun,WANG Rui-long,LIU Yi-na(Zhangzhou Entry-Exit Inspection and Quarantine Bureau,Zhangzhou 363000,China);Extraction of Phoxim in Welsh Onion Under Low Temperature and Its Determination by Gas Chromatography[J];Physical Testing and Chemical Analysis(Part B:Chemical Analysis);2007-06
3 Wu Cheng1,2,Xu Zhiqiang2,Zhang Xiaoli1,Li Guanbin1(1.School of Chemistry and Chemical Engineering,Shandong University,Jinan 250100,China;2.Shandong Agro-environment Protection Station,Jinan 250100,China);Matrix interference and suitability evaluation with multi-residue analysis of organophosphorus pesticides in vegetables[J];Transactions of the Chinese Society of Agricultural Engineering;2007-09
4 LI Ai-jun1,LU Li-jun1,MU Jun1,WANG Ming-tai1,ZHOU Xiao1,ZHANG Yue-chen1,LIU Jing1,YAO Tian-ling2(1.Jilin Entry-exit Inspection and Quarantine Bureau,Changchun 130062,China;2.Changchun Dacheng Maize Development Company,Changchun 130062,China);Determination of Chlorpyrifos Residue in Foods by GC/GC-MS[J];Agrochemicals;2008-11
5 LI Ai-jun1, ZHAO Dong-han2, LU Li-jun1, MU Jun1, ZHOU Xiao1, WANG Ming-tai1, LIU He-ping1, YAO Tian-ling3 (1.Jilin Entry-exit Inspection and Quarantine Bureau, Changchun 130062, China; 2.Jinlin Agriculture University, Changchun 130002, china; 3.Changchun DaCheng Maize Development Company, Changchun 130062, China);Determination of Butachlor Residue in Grains by GC-MS Method[J];Agrochemicals;2009-04
6 LI Ai-jun1,WANG Ming-tai1,MU Jun1,LU Li-jun1,ZHOU Xiao1,LU Chun-mei1,ZHAO Dong-han2,YAO Tian-ling3 (1.Jilin Entry-Exit Inspection and Quarantine Bureau,Changchun 130062,China; 2.Jinlin Agriculture University,Changchun 130002,China; 3.Changchun Dacheng Maize Development Company,Changchun 130062,China);Determination of Multiple Organophosphor Residues in Grains by GC-MS/MS Method[J];Agrochemicals;2009-11
7 LI Si-sheng,LI Jia-tao,LI Chang-an,DAI Zhen(Heifei Center for Disease Control and Prevention,Hefei 230022,China);Determination of twenty organophosphates pesticide multi-residues in vegetables and fruits by capillary gas chromatography[J];Chinese Journal of Health Laboratory Technology;2009-02
Chinese Journal Full-text Database 7 Hits
1 ZHAO Li-feng, XU Lu-mei (Xtaoshan District Sanitation and Antiepidemic Station, Xiaoshan 311200, China);CAPILLARY-GC DETERMINATION OF RESIDUAL ORGANOPHOSPHORUS AND CARBAMATE PESTICIDES IN FRUITS AND VEGETABLES[J];Physical Testing and Chemical Analysis Part B Chemical Analysis;2005-01
2 LIU Chang wu, ZHAI Guang shu, MAI Guang xi, LIU Xiao wei, LIU Feng zhi, CHEN Yong, WANG Yi ru(Agro- Environmental Protection Institute of MOA, Tianjin 300191,China);A Rapid Screen Multiresidue Method for Determination of 27 Organophosphorus Insecticides in Vegetables and Fruits[J];Journal of Agro-environmental Science;2003-03
3 Tang Bo 1) Zhang Jin'e 1) Qi Lihui 2) Cui Guanwei 1) Yin Yanguang 1) ( 1)Department of Chemistry,Shandong Normal University,250014,Jinan,China; 2)Shandong Public Health and Anti-epidemic Station,250014,Jinan,China );NEW PROGRESS OF DETERMINATION OF PESTICIDES RESIDUES BY GAS CHROMATOGRAPHY[J];Journal of Shandong Normal University (Natural Science);2002-04
4 Zhang Bing et al.;Determination of 15 Pesticide Residue in Vegetables by Gas Chromatography/Mass Spectrometry[J];Food Science;2003-08
5 CHEN Hao1,WANG Bao1,WEi Ming-yuan1,XU Juan1,LI Qing1,CHEN Zhi-dong2(1.College of Sciences, Huazhong Agricultural University, Wuhan 430070, China;2.Testing Center, Hubei Academy of Agricultural Science, Wuhan 430064, China);The Application of SPE-GC Method in Residue Detection of Organ Phosphorus Pesticides in Fruits and Vegetables[J];Food Science;2004-10
6 PAN Canping, WANG Limin, KONG Xiangyu, JIANG Shuren, QIAN Chuanfan (Department of Applied Chemistry, China Agricultural University, Beijing 100094 , China);Determination of 15 Organophosphorus Pesticides in Cucumber, Tomato and Pepper Samples by Capillary Gas Chromatography with Gel Permeation Chromatographic Clean-up[J];Chinese Journal of Chromatography;2002-06
7 Lv Yanbai, Wang Xining, Ji Ping. Shangdong Center for Disease Control, Jinan 250014, China;A study on detection of organophosphorous pesticide residues in food[J];Chinese Journal of Health Laboratory Technology;2003-05
Chinese Journal Full-text Database 10 Hits
1 ZHANG Ning (Yibin College, Yibin, Sichuan 646007);Research on the Method of Rapid Testing for Organic Phosphorus Pesticides Residue in Vegetable[J];Journal of Anhui Agricultural Sciences;2005-08
2 PAN Jian et al(Engineering Research Center of Bio-Process of Ministry of Education,Hefei University of Technology,Hefei,Anhui 230009);Pretreatment Method and Installation Research of Pesticide Residue Testing Samples[J];Journal of Anhui Agricultural Sciences;2007-17
3 YAO Xin-jian et al(Department of Chemistry,Zhoukou Normal University,Zhoukou,Henan 466000);Determination on the Organic Phosphorus in Vegetables with Gas Chromatography[J];Journal of Anhui Agricultural Sciences;2008-36
4 GAO Meng-nan,WANG Yan-ping,TANG Hong-wei,LI Bing-qing(Shanghai Environmental Monitoring Centre,Shanghai 200030);Application of Gel Permeation Chromatography to Cleaning up Soil Extracts in Determination of Organochlorine Pesticides[J];Environmental Science & Technology;2006-03
5 WAN Zheng-kai,HE Juan,KANG Chang-an,LU Kui(The School of Chemistry and Chemical Engineering,Henan University of Technology,Zhengzhou 450052,China);Application and Update Progresses of GC-MS in Determination of Pesticide Residues[J];Analysis and Testing Technology and Instruments;2006-01
6 Chen Xiao-Mei*1, Hu Bei-Zhen2,4, Liu Hai-Shan1, Guo Wei-Qiang2, Ding Hui-Ying1, Cen Jun-Jing31(Zhejiang Entry-Exit Inspection and Quarantine Bureau, Hangzhou 310012)2(Department of Chemistry, Zhejiang University, Hangzhou 310028)3(Zhejiang University of Science and Technology, Hangzhou 310012)4 (Shaoxing Entry-Exit Inspection and Quarantine Bureau, Shaoxing 312000);Simultaneous Determination of Carbamate Pesticide Residues in Grains By High Performance Liquid Chromatography-Tandem Mass Spectrometry[J];Chinese Journal of Analytical Chemistry;2007-01
7 LI Sheng-qing 1 ,TIAN Hua 1 ,LIU Xun-cai 1 ,WEI Ming-yuan 1 , CHEN Zhi-dong 2 ,CHEN Hao *1 (1.College of Science, Huazhong Agricultural University, Wuhan 430070; 2.Testing Center, Hubei Academy of Agricultural Science, Wuhan 430064);Residue Analysis of Pyrethrum Ester Pesticides in Cabbage by SPE-GC[J];Journal of Analytical Science;2005-03
8 FU Ruo nong (Department of Chemistry, Beijing Institute of Technology, Beijing 100088),Fenxi Shiyanshi,2003,22(2):94~107;Advances on gas chromatography in China[J];Analytical Laboratory;2003-02
9 Fu Ruo-nong(Department of Chemistry Beijing Institute of Technoligy, Beijing 100081);Advances on gas chromatography in China in recent two years(Ⅱ)[J];Analytical Laboratory;2005-05
10 TANG Fu-bin,CHEN Zong-mao,LUO Feng-jian and Liu Guang-ming(Tea Research Institute China Academy of Agricultural Sciences,Hangzhou 310008);Determination of organophosphorus pesticide residues in tea by solid-phase extraction-gas chromatography[J];Chinese Journal of Analysis Laboratory;2007-02
Chinese Journal Full-text Database 10 Hits
1 Wang Zhiju (The Environmental Protection Bureau of Liuan city ,Anhui province 237000) Wu Xiaodong (The Environmental Research Institute of Xuancheng city ,Anhui province 242000);Applications of Supercritical Fluid Technology in Environmental Protection Field[J];Anhui Chemical Industry;2005-03
2 WAN Yu Anhui Research Institute of Chemical Industry,Hefei 230041,China;The New Development of Sampling Preparation Technique in Pesticide Residue Analysis[J];Anhui Chemical Industry;2006-02
3 ZHANG Pin et al(Shenyang Agricultural University,Shenyang,Liaoning 110161);Multi-residue Determination of NMCs Pesticides in Rice[J];Journal of Anhui Agricultural Sciences;2006-05
4 LIANG Peng et al (Department of Chemical Engineering,Eastern Liaoning University,Dandong,Liaoning 118003);MAE-GC Determination of Organophosphorus Pesticide Residues in Cabbage[J];Journal of Anhui Agricultural Sciences;2007-04
5 ZHANG Chao,CAO Hai-qun,CHEN Li,WANG Jie (College of Plant Protection,Anhui Agricultural University,Hefei 230036);Preliminary Study on the Inhibition of Polysaccharide of Edible Fungi to Plant Virus[J];Journal of Anhui Agricultural University;2005-01
6 TONG Bao-feng 1,2, LIU Ling-hua2, LIU Xiao-ru2, GAO Ji-jun2, ZHOU Huai-dong2, ZHU Duan-wei1(1 College of Resources and Environment, Huazhong Agricultural University, Wuhan 430070, China;2 Department of Water Environment Research, China Institute of Water Resources and Hydropower Research, Beijing 100038, China);Determination of phthalate and adipate esters in the source water by solid-phase extraction and gas chromatography-mass detector[J];Journal of Safety and Environment;2006-02
7 CHEN Shu-shu, XU Kai, XU Yan-jun, PAN Can-ping(College of Science, China Agricultural University, Beijing 100094, China);Determination of honey chloramphenicol residue by monolithic column liquid chromatography-mass spectrometry and QuEChERS purifying method[J];Journal of Safety and Environment;2006-02
8 GAO Hong-qiu~1,SUN Jian~2(1.Agricultural Industrial And Commercial Scientific Research Institute Of Daqing Petrole Management Bureau,Daqing 163316,China;2.Daqing Environmental Monitoring Center Station,Daqing 163316,China);Gas Chromatography Mensurates Multifold Organic Phosphate Pesticide[J];North Environment;2005-06
9 LIU Li-li, CHEN Sha, REN Ren ( College of Environment and Energy Engineering, Beijing University of Technology, Beijing 100022, China );Solid-phase Extraction Pretreatment Technique and Analytic Methods of Organochlorine Pesticides[J];Journal of Beijing Polytechnic University;2003-01
10 SHEN Yan-hua~1 ZHOU Lin~1 CHEN Da-zhou~2 LI Lei~1(1.College of Science,Beijing University of chemical Technology,Beijing 100029;2.National Research Center For CRM'S,Beijing 100013,China);Analysis of organochlorine pesticides in oyster using solid-phase extraction clean-up[J];Journal of Beijing University of Chemical Technology;2005-06
【Secondary References】
Chinese Journal Full-text Database 10 Hits
1 LU Wan-ping1,YOU Fei-ming2,LI Xin1,WU Fang1,ZHANG Lan1(1.Instrumentation Analysis and Measurement Center of Fuzhou University,Fuzhou 350002;2.Fu jian Provincial Central Inspection Institute,Fuzhou 350002,China);Study on Pretreatment Method for Determination of Organochlorine and Pyrethroid Pesticides Residues in Teas[J];Analysis and Testing Technology and Instruments;2009-02
2 SU Jian-feng,HU Chao-yang,CHEN Jin-xing and CHEN Pei-gui(Fujian Fairreach Food Safety Testing Co.,Ltd,Fuzhou 350015);Rapid determination of residual amounts of 103 pesticides in green soy bean by gas chromatography/mass spectrometry[J];Chinese Journal of Analysis Laboratory;2009-06
3 DING Zong-Bo WEI Yi-Shan SUN Ya-Ping(Qingdao Supervision and Test Center for Agriculture Products Quality,Qingdao,Shandong 266109,P.R.China);Determination of Phoxim Residues in Peanut by Vortex-Mixing Extraction and Gas Chromatography[J];Chinese Journal of Spectroscopy Laboratory;2008-06
4 ZHENG Xiao-yan1,LU Wan-ping2,HUANG Hong-xia1,CHEN Jin-quan2,ZHANG Lan2(1Fu jian Provincial Central Inspection Institute,Fuzhou 350002,China;2.Instrumentation Analysis and Measurement Center of Fuzhou University Fuzhou 350002,China);Solid Phase Extraction GC Analysis of Phosphate Pesticide Residue in Vegetables and Fruits[J];Analysis and Testing Technology and Instruments;2009-03
5 ZHOU Fang, SUN Cheng, LIU Hao;Research on Operation Improvement of Solid Phase Extraction[J];Jiangsu Environmental Science and Technology;2008-01
6 YU Jing, ZHOU Zheng-xiang, ZHU Lei, ZHAO Ya-song (Beijing Products Quality Supervision and Inspection Institute, Beijing 100071, China);Development of a GC-NPD Standard Addition Method for Detection of Organo-phosphorus Pesticide Residues in Laboratory Test[J];Agrochemicals;2008-09
7 YING Xing-hua1,XU Xia1,HU Min-jun2,ZHU Zhi-wei1,MIN Jie1,SHI Jian-hua1 (1.Rice Product Quality Supervision and Inspection Center,China National Rice Research Institute,Ministry of Agriculture,Hangzhou 310006,China;2.Fuyang Agriculture Bureau of Zhejiang Province,Fuyang 311400,China);Determination of Thirteen Organophosphate Pesticides Residue in Chinese Chive by Capillary Gas Chromatography[J];Journal of Instrumental Analysis;2009-10
8 CHEN Meng,LU Wan-qing,HAN Yan,HUANG Qun-teng,SUN Guang-da(Environmental Science Research Center,College of Oceanography and Environment,Xiamen University,Xiamen 361005,China);Simultaneous Determination of 36 Pesticides in River Water and Sea Water Using Solid Phase Extraction-Gas Chromatography[J];Journal of Instrumental Analysis;2009-12
9 QIN Long1,YANG Meng-qi2,WANG Jian-ying1,JIANG De-quan2,WEI Yan-hua2,WANG Yang-ju2,BU Cheng-yi2,YAN Xing-feng2,DING Rui-chao2 (The Epidemic Prevention Team of the GED of PLA,Beijing 100101,China);Determination of organophosphorus pesticide multi-residues in vegetables and fruits by capillary gas chromatography[J];Chinese Journal of Health Laboratory Technology;2010-01
10 QIN Long,YANG Meng-qi,WANG Jian-ying,et al. (The Epidemic Prevention Team of the GAD of PLA,Beijing,100101,China);Determination of Multi-residues of Organophosphorus Pesticides in Vegetables by Capillary Gas Chromatography[J];Occupation and Health;2010-02
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 Yu Xiaoying; Lei Sheng(Institute of Geochemistry, Chinese Academy of Sciences, Guiyang 550002)Chen Guichun(Sanitary and Anti-epidemic Station of Cuizhou Province);A Biosensor Prepared by Coating Acetyl Choline Esterase Membrane on Ion Selective Field Effect Transistors[J];Chinese Journal of Analytieal Chemistry;1996-05
2 Zhong Weike; Hao Jian; Fan Yaobo; Wang Minjian (Research Center for Eco-Environmental Sciences, Chinese Academy of Sciences, Beijing 100085);Development in Pesticide Residues Analysis of Food[J];Chinese Journal of Analytieal Chemistry;2000-07
3 Zhang Weihao, Xu Xiaoqing  (Institute of Hydrobiology, Chinese Academy of Sciences, Wuhan 430072);Determination of Trace Level Microcystins in Water Using Solid-phase Extraction and High Performance Liquid Chromatography[J];Chinese Journal of Analytieal Chemistry;2001-05
4 Li Jinpei (Yunnan Institute of Tobacco, Yuxi 653100);Determination of Pyrethrums Residue in Tobacco by Wide-Bore Capillary Gas Chromatography[J];Chinese Journal of Analytieal Chemistry;2001-07
5 Ren Jin, Huang Cuiling, Zhao Guodong, Jiang Ke  (Research Center for Eco Environmental Science, Chinese Academy of Sciences, Beijing 100085);Determination of Herbicides in Drinking Water by Solid Phase Extraction-Liquid Chromatography-Mass Spectrometry[J];Chinese Journal of Analytieal Chemistry;2001-08
6 Zhang Yuming Ho Yunhan(Institute of Pharmacology and Toxicology,Academy of Military Medical Sciences);DETERMINATION OF ORGANOPHOSPHORUS PESTICIDES BY IMMOBILIZED ACETYLCHOLINESTERASE NYLON NET[J];Environmental Chemistry;1986-06
7 Li Zhixiang, Zhai Yanlu (Environmental Protection Institute, Ministry of Agriculture, Animal Husbandry and Fishery);DETERMINATION OF PESTICIDE RESIDUES IN VEGETABLES AND FRUITS USING A PLANT-ESTERASE INHIBITION TECHNIQUE[J];Acta Scientiae Circumstantiae;1987-04
8 Ta Na; Tian Weiping; Zhang Zhijuan and Zhang Xiufang(Department of basic Curriculum, Inner Mongolia Institute of Agriculture and Animal Husbandry);SURVEY OF ORGANIC PHOSPHORUS PESTICIDE RESIDUES IN VEGETHBLES GROWN IN SHED[J];Journal of Inner Mongolia Institute of Agriculture and Animal Husbandry;1997-03
9 Li Chongjiu; Fei Jing; Liu Jianpo (College of Fundamental Science & Technology);Study on Pesticides Multiresidue Analyses in Cucumber by GC/MS (MID)[J];JOURNAL OF CHINA AGRICULTURAL UNIVERSITY;1998-03
10 Yang Manjun(Huanan Agricultural University,Guangzhou 510642);The New Extraction Techniques in Pesticide Residue Analysis[J];Pesticide Science and Administration;2000-01
©2006 Tsinghua Tongfang Knowledge Network Technology Co., Ltd.(Beijing)(TTKN) All rights reserved