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《Liaoning Chemical Industry》 2009-01
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Preparation of Molecularly Imprinted Polymer with Racemic Cefradine as Template and Study on Its Chiral Resolution

XING Zhan-fen1,2,CHENG Hong-da1,ZHENG Yan1,SU Li-qiang2 (1.Shandong Wanjie Medical collage,Zibo 255213,China;2.Qiqihar University,Qiqihaer 161006,China)  
The molecularly imprinted polymer(MIP) was prepared with racemic Cefradine as template and synthesized(S)-(1-phenylethyl)-methlacrylamide as chiral functional monomer.The selective recognition ability of MIPs was studied by high performance liquid chromatography(HPLC).The molecularly imprinted polymers as stationary phase has good chiral resolution ability to Cefradine enantiomers.Three Racemic amino acid ramification molecularly imprinted polymers were prepared by the same method,but the relevant substances did not get resolution.the comparison showed: If preparation of molecularly imprinted polymer with racemic cefradine as template is carried out,the template molecules needs four function places at least.
【Fund】: 黑龙江省教育厅科学技术研究项目(11511435)
【CateGory Index】: O631.3
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