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《Refractories》 2002-06
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Research on synthesizing technique of β'-Sialon material by nitridation reaction

Cao Linhong,Jiang Mingxue  
β'-Sialon materials were synthesized by nitridation reaction with metallic silicon powder,aluminum powder and alumina powder as starting materials.The nitridation technique systems,including (1) from room temperature to 600 ℃ at 10 ℃·min -1,600 ℃ to 700 ℃ (holding for 2.5 h) at lower than 2 ℃·min -1 and (2) from room temperature to 1200 ℃ at 10 ℃·min -1,1200 ℃ to 1350 ℃ (holding for 6 h) at 2 ℃·min -1,with flowing nitrogen as furnace atmosphere and flow rate lower than 0.2 m 3·h -1,for preparing β'-Sialon materials with different Z-values were researched. The results indicate that the nitridation rate of all of the specimens are more than 80%,showing the nitridation technique systems are reasonable.XRD analysis results reveal that β'-Sialon phase primarily exists in the final product after nitridation,a small amount of α-Al 2O 3 and 15R polytypoid phase remains in the specimens with high Z-values.β'-Sialon phase in the sintered specimens shows hexagonalprism-like microstructure.
【CateGory Index】: TQ175
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