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《Journal of Lanzhou University(Medical Sciences)》 2010-02
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Determination of icariin in Shenqibolikang tablets by high performance liquid chromatography

BAI Zhong-mei~1,WEI Xue-bing~2 (1.Department of Pharmacy,General Hospital of Jingyuan Coal Industry Group Ltd,Baiyin 730913, Gansu,China;2.Gansu Province Institute for Drug Control,Lanzhou,730000,China)  
Objective To set up a method for determining the content of icariin in Shenqi-bolikang tablets.Methods The separation was performed by high performance liquid chromatography in a ZORBAX SB-C_(18)column(250 mmx4.6 mm,5μm)with a mobile phase of V(acetonitrile):V(water)=30:70.The flow was 1.0 mL/min and the detective wavelength was set at 270 nm.Results The standard icariin showed a good linear correlation within the range 0.063~1.58μg.The average recovery of the loading was 97.1%and the relative standard deviation was 0.83%.Conclusion This method can be used for quality control of the icariin in Shenqibolikang tablets.
【Key Words】: high performance liquid chromatography Shenqibolikang tablet icariin
【CateGory Index】: R286
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【References】
Chinese Journal Full-text Database 1 Hits
1 WU Hong-ling(Hospital of traditional chinese medicine of hengyang,Hunan Hengyang 421001);Were determined by HPLC method for summer in winter disease shot barrenwort content[J];Guiding Journal of Traditional Chinese Medicine and Pharmacy;2011-08
【Citations】
Chinese Journal Full-text Database 7 Hits
1 ZHAO Li-dong1,2,ZHANG Hua-feng2,3,DONG Jing-zhou2,3 and WANG Ying2(1.College of Life Science,Huazhong Normal University,Wuhan 430079,China; 2.Wuhan Botanical Garden,Chinese Academy of Sciences,Wuhan 430074,China; 3.Graduate University of Chinese Acadmy of Sciences,Beijing 100049,China);Ultrasonic-assisted Extraction of Icariin from Epimedium macranthum Leaves and Their Stability[J];Acta Agriculturae Boreali-Occidentalis Sinica;2007-06
2 ZHI Yue-fang,ZHANG Chi-bing,ZHOU Ping.Department of Pharmaceutics,Jiangsu Provincial Hospital of Traditional Chinese Medicine,Nanjing 210029,China;High-performance liquid chromatographic determination of icariin in jujing pills[J];Chinese Remedies & Clinics;2004-05
3 YANG Fan(College of Pharmacy,Guangdong University of Pharmacy,Guangzhou 510224,China)ZHONG Guixiong(Liming Pharmaceutical Factory,IVZON Pharmaceutical Group Inc,Shaoguan 512028,Ch_ina)ZHAO Hongpu(The Guangdong Hospital of TCM,Guangzhou 510000,China)LIN Chunyan,WEN Xiaoqing,HE Xiaoling(2000 Grad in College of Pharmacy,Guangdong University of Pharmacy, Guangzhou 510224,China);Orthogonal Design Experiment on the Extracting of Icariin by Different Means[J];China Pharmacy;2005-06
4 WANG Xin, WANG Ting-ting, WANG Hai-jun, WENG Dai-qun, YANG Yong, LI Qing, LUO Wei-zao(Chongqing Academy of Chinese Materia Medica, Chongqing 400065, China);Optimization of the Extraction Technology of Icariin from Herba Epimedii[J];China Pharmacy;2009-09
5 Yi Xuefu (Huayuan Pharmaceutical Ltd., Jingjiang City, Jiangsu Province, 214500);Determination of Icariin in Huorong Bushen Granules by HPLC[J];Chinese Pharmaceutical Affairs;2004-07
6 WANG Ming-quan 1, BI Zhi-ming 1, LI Ping 1, JI Hui 1, CHENG Fei-long 2 (1.Department of Pharmacognosy, China Pharmaceutical University, Nanjing 21003 8 ,Jiansu, China; 2.Zhejiang Zuo Li Pharmaceutical Co. Ltd., Huanzhou 313200, Zhejiang , China);Determination of Epimedin C and Icariin in Herba Epimedii by HPLC[J];China Journal of Chinese Materia Medica;2003-11
7 YANG Liu1, ZHONG Jingxian1, LIN Qiaolin2, XIE Peishan2, HUANG Haiyan1( 1. Guangdong Provincial Hospital of TCM, Guangzhou 510120; 2. Guangzhou Institute for Drug Control, Guangzhou 510122);Studies on Extraction of Icariin in Herba Epimedii[J];Traditional Chinese Drug Research & Clinical Pharmacology;2005-04
【Co-citations】
Chinese Journal Full-text Database 10 Hits
1 LI Qing-jie et al(Jilin Tianyao Technology Co.,Ltd,Changchun,Jilin 130012);Study on Extraction of Compound Luronggubao Capsule[J];Journal of Anhui Agricultural Sciences;2011-12
2 JIANG Ling-yun1,LIU Guang-ming1,CHEN Ke-xin2 1.School of Pharmaceutical and Chemical,Dali University,Dali 671000,China 2.School of Basic Medicine,Dali University,Dali 671000,China;Advances in study on icariin extraction,separation,and its anti-tumor mechanism[J];Drugs & Clinic;2011-05
3 BAO Ru-po,ZHAO Hao-ru,LU Chun-tao(Department of Pharmaceutics of TCM,China Pharmaceutical University,Nanjing 210038,China);Studies on Drying Process of Fufang Qiangshen Granules by Spray Drying Method[J];Strait Pharmaceutical Journal;2006-03
4 ZHAO Ming-hong,HAN Juan-zhu,WANG Chang-li,FAN Dong-jiao Department of Pharmacy,The General Hospital of Shenyang Military Region,Shenyang 110840,China;Simultaneous Determination of Icariin and TanshinoneⅡ_A in Fufang Xianlingpi Granula by High Performance Liquid Chromatography[J];Pharmaceutical Journal of Chinese People's Liberation Army;2011-01
5 YAO Huijuan,HU Daode,GU Lei,WANG Songpo,LIU Gaolin(Department of Clinical Pharmacy,The First People' s Hospital,Shanghai Jiaotong University,Shanghai 200080,China);Determination of icariin in Herba Epimedium by reversed-phase high performance liquid chromatography[J];Chinese Journal of Clinical Pharmacy;2010-01
6 LI Kun-feng1,2,LI Xiao-long1,2,CAO Pei-xue2,PAN Wei-dong2,HE Shun-zhi1,LIANG Guang-yi1,2(1.Guiyang College of Traditional Chinese Medicine,Guiyang 550002,Guizhou,China;2.The Key Laboratory of Chemistry for Natural Products of Guizhou Province and Chinese Academy of Sciences,Guiyang 550002,China);Content Variation of 2 Mainly Components in Leaf of Epimedium of Different Areas and Maturity Stage[J];Liaoning Journal of Traditional Chinese Medicine;2011-08
7 LIU Min,ZHOU Fang,HUANG Shao-wei,CHI Ru-an~*,WU Yuan-xin,WANG Cun-wen,JU Xiu-lian,GUO Jia,HUANG Qi-mao(Hubei Key Lab of Novel Reactor &Green Chemical Technology,Wuhan Universiby of Engineering,Wuhan,430073,China,);The Extraction Technology for Total Flavone and its Content Distribution in Herba Epimedium[J];Lishizhen Medicine and Materia Medica Research;2007-01
8 ZHU Sheng,OU Hai-jun,ZHAO Shu-er,ZUO Hua-ting,ZHU Jin-long(Zhejiang Newcovery Biotech Co.,Ltd,Zhejiang Ningbo 315800,China);Determination of Icariin Epimedium from Different Haital in China by HPLC[J];Lishizhen Medicine and Materia Medica Research;2008-09
9 ZHANG Hua-Feng1,2,GAO Xiang1,2,LU Da-yan1,WANG Ying1(1.Key Laboratory of Plant Conservation Genetics,Wuhan Botanical Garden,Chinese Academy of Sciences,Wuhan 430074,China;2.Graduate School,Chinese Academy of Sciences,Beijing 100049,China);Simultaneous Determination of Epimedin A,B,C and Icariin in Herba Epimedii by High Performance Liquid Chromatography[J];Journal of Instrumental Analysis;2007-02
10 ZHAN Pei-ying1,LI Gui-juan2(1.Department of Chemistry,Tonghua Normal University,Tonghua,Jilin 134002,China;2.College of Chemical Engineering,Changchun University of Technology,Changchun,Jilin 130012,China);Optimum Conditions of Extracting Icariin by Microwave Method[J];Journal of Tonghua Normal University;2010-10
【Co-references】
Chinese Journal Full-text Database 1 Hits
1 OU Ji-ming1,DENG Rui-yun1,CHEN Yong-gang1,2,ZHOU Gai-lian1,LIN Li1,3,CHENG Chen-bo3,LI Ming3 (1.School of Chinese Materia Medica,Guangzhou University of TCM,Guangzhou,Guangdong 510006,China;2.Affiliated People's Hospital of Yunyang Medical College,Shiyan,Hubei 442000,China;3.Hironaka Institute of Marine Drug and Functional Foods,Guangzhou,Guangdong 510006,China);Determination of icariin in Naoyiyuan capsules[J];Journal of Guangdong Pharmaceutical College;2010-01
【Secondary Citations】
Chinese Journal Full-text Database 10 Hits
1 LI Hui , WANG Jian-feng (Dalian Nationalities University, Dalian Development Zone 116600, China);The Extraction and Content Determination of Alkaloids from Aconitum Kusnezoffii[J];Journal of Dalian Nationalities University;2002-01
2 Guo Baolin; Xiao Peigen (Institute of Medicinal Plant Development,Chinese Academy of Medical Sciences Beijing l00094);DETERMINATION OF FLAVONOIDS FROM EPIMEDIUML.IN SICHUAN[J];WEST CHINA JOURNAL OF PHARMACEUTCAL SCIENCES;1996-02
3 NIE Ling Yun ①,CHEN Zhi Sheng ② ( ① Institute for Drug and Instrument Control Health Dept GLD of PLA.Beijing 100071) ( ② Depa rtment 59823 of PLA.Beijing 100071);HPLC Determination of Icarrin in Qianlie Shule Keli[J];PHARMACEUTICAL JOURNAL OF CHINESE PEOPLE'S LIBERATION ARMY;2000-05
4 GUO Xiao_wu(Applied Acoustics Institute, Shaanxi Normal University, Xi′an 710062, Shaanxi, China);Result of Epimedic Sagittaum leaves by ultrasonic extraction[J];Journal of Shaanxi Normal University(Natural Science Edition);2002-04
5 ZHU Chun-lin, GAO Su-qin (Changzhou Traditional Chinese Medicine Hospital, Changzhou 213003, Chi na);Optimization of Extraction Process of Herba Epimedii[J];LiShiZhen Medicine and Materia Medica Research;2001-08
6 BL Guo;CL Wang;JM Chen and PG Xiao(Institiute of Medicinal Plant Development, Chinese Academy of Medical Sciences and Peking Union Medical Sciences and Peking Union Medical College,Beijing 100094);DETERMINATION OF 9 FLAVONOIDS IN 5 SPECIES OFEPIMEDIUM RECORDED IN CHINESE PHARMACOPOEIA BY HPLC[J];ACTA PHARMACEUTICA SINICA;1996-04
7 Guo Baolin;Wang Chunlan;Xiao Peigen(Institute of Medicinal Plant,chinese Academy of Medical Sciences,Chinese Xiehe Medicl University,Bejing0;Determination of Flavonoids and Quality Evaluation of Sagittate Epimedium(Epimedium sagittatum)[J];Chinese Traditional and Herbal Drugs;1996-10
8 Institute of Medicinal Plants, Chinese Academy of Medical Sciences & Peking Union Medical College (Beijing 100094) Wang Yuping and Guo Baolin;Quantitative Analysis of Total Flavonoids and Icariin in “Xianlinggubao Capsule”[J];CHINESE TRADITIONAL AND HERBAL DRUGS;2000-10
9 LIU Gui-xia 1, NI Yan 2, SU Qiang 2, LIU Zhen-quan 2, LI Xian-rong 2 (1 Tianjin College of TCM, Tianjin 300193, China; 2 Shanxi Academy of TCM, Taiyuan Shanxi, 030012, China);Studies on standard for quality control of QISHEN CAPSULE[J];Chinese Traditional and Herbal Drugs;2001-12
10 XU Jiandong,WANG Hongquan,ZHANG Wenying,WU Meizhen(Tongji Hospital of Tongji University,Shanghai200065);Influence of Different Composed Herbs and Decocting Processes on Content of Aconitine in Rhubarb and Aconite Decoction[J];China Pharmacy;2003-10
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