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《Journal of Nanjing University of Science and Technology》 2004-01
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Studies of Vessel Explosion Prevention in the Synthesis of AgGaS_2 Polycrystalline

ZHANG Wei, ZHU Shi-fu, ZHAO Bei-jun, WANG Rui-lin, LIU Ming-wen, LI Yi-chun(Department of Material Sciences, Sichuan University, Chengdu 610064, China)  
This paper presented a new procedure of AgGaS_2 polycrystalline synthesis via analyzing and exploring the reasons of explosion during the synthetic processes in the vessel chamber. The new procedure includes those steps such as two-temperature-zone vapor transportation and temperture oscillation. The new method synthesized high purified and polycrystalline AgGaS_2 with Single phase. Explosion was successfully avoided due to the reduction of pressure in the synthetic chamber. Single crystal AgGaS_2 was obtained with a size of φ10×15mm by Bridgman's method using the synthetic AgGaS_2. XRD was used to characterize those synthetic materials and the results proved that synthetic AgGaS_2 was polycrystalline with single phase.
【Fund】: 四川省应用基础研究基金(99-479)
【CateGory Index】: TQ08
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